GCMS analysis results for sample AE06449, April 2002

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1702\6449.D Vial: 7 Acq On : 17 Apr 2002 2:06 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 36.09 0.86 ug/1 66783 Perylene-dl2 37.87 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane, 1,1,1, ,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 38 2 3-Trimethylsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 32 3 3-Isopropoxy-1,1,177,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 4 Mercaptoacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 17 Abundance Scan 3381 (36.087 min): 6449.D (-) m/ z 73.00 100.00%] 73

147 5000 221 281 355 429 35.80 36.00 36.20 36.40 40 । 191/ 253 i 327, , 401 1 —— TFIIT ,1,1,I I, I I I TT—+ i 1 ■ 1 ■ i1 ' ‘ 1 1 I I 1I ,2 T I I J I I I I I I TT 1 m/z 147.00 53.59% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 / 5000 A AA 281 35.80 36.00 36.20 36.40 m/z 221.05 36.19%| 45 369 1 ■ i ' 1 117 , 207 249 ■ ■ i ■ ■ ■ ■ i ■ ■ TI—0—*——1—n——O—I—BTPCCIT mlz—> 50 100 150 200 250 350300 400 450 500 550 Abundance #56734: 3-Trimethylsilyloxystearic acid, trimethylsilyl est 73 T■ I 1 1 1 1 | 1 > 35.80 36.00 36.20 36.40 5000 147 233 m/z 355.05 25.30%l

313 429 189 [339 387

mz—> -—r ,• L। ■ ■ i ■ ■ । • ■ ■ ■ 1 ■ ' ■ I 1 > 50 100 150 200250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 11 1 1 ' 1 1 1 1 1 73 35.80 36.00 36.20 36.40 m/z 281.05 20.69%

5000 147

221 281 . I...I . 327 1 1 । 1 1 1 1 । ■ 1 1 1 । ' ‘ 1 1 । 1 ' 415 519 561 m/z—> 50 100 150 200 250 300 350 400 450 500 550 35.80 36.00 36.20 36.40

6449.D GCMS0412.M Thu Apr 18 09:10:58 2002 Page 15

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