GCMS analysis results for sample AE04805, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2802\4805.D Vial: 20 Acq On : 29 Mar 2002 3:23 am Operator: Sample : gc/ms scan 3/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L’

Peak Number 6 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

45.55 1.57 ug/1 87635 Perylene-dl2 37.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3,6-Dioxa-2,4,5,7-teti7&silaoctane, 294 C10H3002Si4 004342-25-0 43 2 Trisiloxane, 1,1,1,5/5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 12 3 Tris(trimethylsilyyborate 278 C9H27BO3Si3 004325-85-3 10 4 Trisiloxane, octamethyl- 236 C8H24O2Si3 000107-51-7 10 Abundance Scan 4412 (45.547 min)“: 4805.0 (-) 7)3 147 221

281 5000 355

429 44 I, r.. Ij. m ffT.T, 1931 I...,, , 11.1 ,-T I . p . .. I 253. , Il LI I" " r'' J" ' 1 45.20 45.40 45.60 45.80 m/z 146.95 96.46% m/z~>____ 40_ 60.. 80 100120140 160 180 200 220 240 260 280 300 320 340 360 380400 420 Abundance #41682:3,6-Di6xa5’4X74etrasiiaoctah¥”^ .. 147 2ii

73 A .. 5000 45.20 45.40 45.60 45.80 191 117 279 m/z 221.0.5 88.46% I I I I __ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #52459: Tnsiloxane, i’.5.5.5-!iexarnetliyl-3.3-bis[(tnrnet 73 147 i 281 45.20 45.40 45.60 45.80 _ 5000 m/z 281. Oh 53.66% 369 27 249 338 7n/z-> 40 60.80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 'Abundance #39028: Tris(trimethylsilyijborate 7)3 221 45.20 45.40 45.60 45.80_____ ! m/z 355.05 46.74% 5000 I 263 133 ■I I 175 I 1 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 45.20 45.40 45.60 45.80 ■

4805.D GCMS0308.M Mon Apr 01 15:49:43 2002 Page 6

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