TCLP calibration table review document, April 2002

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Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.

NYC-WTC_000043262–000043272

Folder label: “GCMS X 4/22/02 A 5/3/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1702\8209.D Vial: 20 Acq On : 18 Apr 2002 2:46 am Operator: Sample : gc/ms scan 4/8 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 38.51 2.85 ug/1 467757 Perylene-dl2 37.88 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3,6-Dioxa-2,4,5/7-tetrasilaoctane, 2 94 C10H3 002Si4 004342-25-0 46 2 Trisiloxane, 1,1, 1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 22 3 Tris (trimethy ilyl)borate 278 C9H27BO3Si3 004325-85-3 14 4 3-Isopropoxyy ,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 12 Abundance C Scan 3645 (38.511 min): 8209.D (-) m/z 73.00 100.00% . 73 147 221

5000 281 355

429I i I | i I । i pi m i | i । > । | i ii t ।

38.20 38.40 38.60 38.80

m/z-> 44 TT 96 i, । dreuil) ।11,111 1931

TWTTTTTT ' r '"i 11"T‘11 i it| 327 1 ii I ।" " 1 40 60 80 100120140160180200220240260280300320340360380400420 TTTTTT 263 1, 4014L - m/z 147.00 84.26% Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 147 2121

W 5000 38.20 38.40 38.60 38.80 191 m/z 221.05 77.41% 117 279 1" " 1 TTT r11' 1 ........ ..................................... TTL p i i i । i । । । । । । i i J i r । i j i । [ i | | | | | | | | | | | I I I I ] I I H | I I TTTTTT m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147

5000 m/z 355.00 44.20% 281 45 369 117 207 249 ’' I'1" I" " 11 i" " i •1'1 r“" i 100000000103111 । i i i i 11 i i i । i i i i । i i r i 11 ri p i i 11 j i i i i j ri i i ।

m/z-> 40 60 80 100120140160180 200220240260280300320340360380400 420 Abundance #39028: Tris(trimethylsilyl)borate I I I » I I I [ I I I I I I 1 I I—I I—I—I—I—s 73 221 38.20 38.40 38.60 38.80 m/z 281.00 43.97% _/ 5000 263 133 175 ,1 1..... L p 1 " [> " l p 1 1 I p H 1 p " 1 p "I p 1 1 1 p " l| 1II m/z-> 40 60 80 100120140160180 200220240260280300 320340360380400420 38.20 38.40 38.60 38.80

8209.D GCMS0412.M Thu Apr 18 14:11:06 2002 Page 2

NYC-WTC_000043268

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GCMS analysis results for sample AE06456, April 2002 · Box DEP Box 23

NYC-WTC_000039611

Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.

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