TCLP calibration table review document, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1702\8209.D Vial: 20 Acq On : 18 Apr 2002 2:46 am Operator: Sample : gc/ms scan 4/8 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1-Monolinoleoylglycerol trimet Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 38.75 0.97 ug/1 159917 Perylene-dl2 37.88 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 23 2 3-Isopropoxy-1,,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 23 3 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 22 4 N-(Trifluoroabetyl)-N,O,O' ,0''-tetr 553 C22H42F3NO4Si4 000000-00-0 9 Abundance Scan 3671 (38.749 min): 8209. D (-) m/z 73.00 100.00% 73

147 5000 221 355 281 11 1/7 i n ] i i i i-1 i i i l i-1 i i । r 429 38.40 38.60 38.80 39.00 I , 191 i i ] i 1 i । i ! r । । । r-1 f pi r 1—" 249 L} 325, 1 i ‘ h I ■ 1tT 1401W.... 11 I I I I I T I | I I T m/z 147.00 62.52% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871:1 -Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 — 38.40 38.60 38.80 39.00 34 103 m/z 221.05 47.54% 281

m/z—> 50 100 . 200 . 150 ___ 395,111/482 __ 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

38.40 38.60 38.80 39.00 5000 m/z 355.05 27.92% 147 /,

m/z—> . 271 21327 i " 1 k 1 J 1 । । l i । । । | i <1 । | । । it । i C T i । ।—।—।—rm—।—।—।—।—।—i—।—।—0—।—।—[—।—r 50 100 150 200 250 300 350 400 450 500 415 519 550561 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 38,40 38.60 38.80 39.00 147 m/z 207.00 26.58%

5000

45 1 ' i 1 1 117- "I I I I 11 I 207 I I I I I 249 r1 281 369 1 1 | । । । । | > i i I | । i i i | | । i , [ |—i—i—i—।—i—r _A_ 1 I 'I I I I I ] I I I I ] I I I I d I I I I I m/z-> 50 100 150 200 250 300 350 400 450 500 550 38.40 38.60 38.80 39.00

8209.D GCMS0412.M Thu Apr 18 14:11:08 2002 Page 3

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