GCMS analysis results, sample AE04947, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR3002\4947.D Vial: 14 Acq On 30 Mar 2002 3:51 am Operator: Sample gc/ms scan 3/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Monolinoleoylglycerol trimet Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

36.14 0.70, ug/1 47080 Perylene-dl2 37.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 37 2 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 17 3 3-Isopropoxy- ,1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 17 4 Trisiloxane, ,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 16 Abundance Scan 3387 (36.136 min): 4947.D (-) m/ Z 713

147 5000 221 281 355 429 35.80 36.00 36.20 36.40__ _ 44 4^ 327, '\ ' I ' .... . m/z. 147.00 ' 55.36% 'm/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoyiglycerol trimethyisilyl ether 73

207 5000 147 ...........1 / I , I ? , I I 35.80 36.00 36.20 36.40 34* I 103 . ; 281 m/z 221.05 ■ 39.64%

m/z-> ! -JU-M 50 100 150 200 250 , 1 300 350 400 . , , , , 482 450 500 , I , , 550 Abundance #56714: 1.1.1 .S.r./.Z-HeptaiTietnyl-a.S-bisitnnicthylsiioxyjt 73

147 35.80 36.00 36.20 36.40 5000 267 m/z 355.05 23.80% 355 429 45 ■ 207 • I , ,1 ..... 50 100 150 200 250 300 350 400 450 500 550 Abundance' #66503: 3-isopropoxy-i,i,1,7,7,7-hexamethyl-3,5,5-tris(trim 713 _ 35.80 36.00 36.20 36.40 ____ m/z 207.00 21.19% 5000 147

281 327 415 I 1 [ ~I I I 519 561 50 100 150 200 250 300 350 400 450 500 550 35.80 36.00 36.20 36.40

4947.D GCMS0308.M Tue Apr 02 11:10:22 2002 Page 2

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