GCMS analysis results for sample AE04411, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2502\4411.D Vial: 17 Acq On : 26 Mar 2002 1:59 am Operator: Sample : gc/ms scan 2/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1-Monolinoleoylglycerol trimet Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

36.14 10.49 ug/1 794313 Perylene-dl2 37.94

Hit# of 5 Tentative ID MW MolForm, CAS# Qual

1 1 -Monolinoleoylglycerol trimethylsi 498 C27H54O4S 2 054284-45-6 25 2 Silanamine, N- [2, 6-dimethyl-4-[ (tri 281 C14H27NOS12 072088-09-6 18 3 1,1,1,5,7,7,7-Jieptamethyl-3,3-bis (t 444 C13H40C5Si6 038147-00-1 17 4 3-1sopropoxy- ,1,1,7,7,7-hexamethyl 576 C18H52C7Si7 071579-69-6 12 Abundance Scan 3387 (36.140 min): 4411.D (-) m/z 73.00 1 00.00% 73 147 5000 221 281 355 i i । । i i i |"i r ■ > । 11s"Il"l i i | 1 I 429 35.80 36.00 36.20 36.40 45 ' ‘1 1 t 96 117.. , Wlj 249, 1 J , 327, 1 , , 401, m/z 146.95 57.38% miz-> 50 100 150 200 250 300 350 400 450 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73 207 5000 147 - 1 1 | T ■ T 1 | ,, rm—en I I I ■ | 35.80 36.00 36.20 36.40 34 103 281 m/z 221.05 42.15% 395 1 • i • ■ 4 482 m/z-> 50 100 150 200 250 300 350 400 450 Abundance" ' moner nine PG- ’ .1 !0n - : ailylaconyi 73 281 LDdCTt////1/1/n/n.T 209 35.80 36.00 36.20 36.40 5000 m/z 281.05 23.95% 45 251 . 179 125147 ;

miz-> 50 100 150 200 250 300 350 400 450 Abundance #56714:1,1,1,5,7,7,7-Heptamethyi-3,3-bis(trimethylsiloxy)t 73 35.80 36.00 36.20 36.40 m/z 355.05 22.51% 147 5000 267 355 429 207

1 45 ‘I .....IJ.... 1 1 ‘ I ‘ ‘ ‘ I ' ' ‘ ' I ' ' ' ‘ I ‘ m/z-> .50 100 150 200 250 300 350 400 450 35.80 36.00 36.20 36.40

4411.D GCMS0308.M Thu Mar 28 12:33:49 2002 Page 3

NYC-WTC_000011886