GCMS analysis results for sample AE04411, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR25O2\4411.D Vial: 17 Acq On : 26 Mar 2002 1:59 am Operator: Sample : gc/ms scan 2/28 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L **************************************************************** ***** Peak Number 4 1-Monolinoleoylglycerol trimet Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

37.38 26.12 ug/1 1978390 Perylene-dl2 37.94

Hit# of 5 Tentative ID MW MolForm/) CAS# Qual 1 1-Monolinoleoylglycerol trimethylsi 498 C27H540 4Si2 054284-45-6 25 2 1,1,1,5,7,7 ,7-H:eptamethyl-3,3-bis (t 444 C13H40d5Si6 038147-00-1 20 3 3-1sopropoxy-1,1, 1,7,7,7-hexamethyl 576 C18H5207Si7 4 1,2 -Benzenedicarboxylic acid, bis(t 310 C14H2204Si2 Abundance Scan 3522 (37/379 min): 4411.D H " " 73 147 " iml— 7TT 071579-69-6 002078-22-0 12 10

5000 221 281 355 ■ I ‘ ■ I ‘ ‘ ‘ ‘ I ‘ ‘ ' ‘I’-' * ‘ I • 429 37.00 37.20 37.40 37.60 37.80 45 117 191,1 । 2249 , ( . 327. 1 401 1 1 1 ''1 1 1 TFr PTiFi fui 4 f.h . .1 11 I .'i t* r। । । r m/z 146.95 63.61% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73 207 5000 147 ‘ I* 37.00 37.20 37.40 37.60 37.80 34 103 m/z 221.05 48.28% 281 482 395 dl 1**I‘‘"+I‘‘‘I‘‘‘‘I‘*‘*I****1****I** miz-2 50 100_ 150. 200 250 300 350 400 450 500 550 Abundance f : 1 ' r • Saptetid $ : " 1 73

147 37.00 37.20 37.40 37.60 37.80 5000 267 m/z 281.05 28.45% 355 429 45 207

m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73 m/z 7 77% 37.00 37.20 37.40 37.60 37.80

5000 147 221 281 327, 415 519 561। ‘*1*‘‘I‘‘*I‘IISTIII rru ]■ > ■ ■ < i > ‘ I ■ h 1 । । । । i । । . ■. i . । m/z-> 50 100 150 200 250 300 350 400 450 500 550 37.00 37.20 37.40 37.60 37.80

4411.D GCMS0308.M Thu Mar 28 12:33:54 2002 Page 4

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