GCMS sample analysis results for AE01964, March 2002

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Laboratory report detailing the analytical results for sample AE01964 obtained via GCMS on March 22, 2002.

NYC-WTC_000010332–000010341

Folder label: “GCMS X 1/27/02 A 2/26/02 - 3/5/02 3/20/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR1902\1964.D Vial: 10 Acq On : 20 Mar 2002 7:59 am Operator: Sample : gc/ms scan 3/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Monolinoleoylglycerol trimet Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

38.85 0.40 ug/1 50697 Perylene-dl2 37.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1 -Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 37 2 3-Isopropoxy-1,1,1,7,7, 7-hexamethyl 576 C18H5207Si7 071579-69-6 10 3 Mercaptoacetic acid; bis(trimethyls 236 C8H20O2SSi2 006398-62-5 10 4 2 -Methoxyphenylpyruvic acid, di-TMS 338 C16H2604Si2 000000-00-0 10 Abundance in 3683 (38.852 min): 1964.D (-) m/ z 73.00 100.00% 73 147 5000 221 281 355

J 193 327 429 38.60 38.80 39.00 39'20 ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■i ■ ■ ' • i ■ r■ ■ i • ■ ■ ■ i ■ ■ ■ r r1 1 1 1 i ----- m/z 146.95 56.71% m/z-> 50 100 150__200__ 250 .300. 350.. 400 __450.. 500.. 550 Abundance .......... . . #58871:1-Monoiinoteoylgiycerol trimethylsilyl ether 73

5000 147 207 MAAwww 38.60 38.80 39.00 39*20 34 103 281 m/z 221.05 44.24%

m/z->__ 50 100 150 200 250 300 350 395, .482 400 450 500 550

n Abundance 73 T-r-j-r-r ‘ ' I ' ‘ ‘ ‘ I ‘ ‘ 38.60 38.80 39.00 39.20 5000 147 m/z 281.05 27.98% 221 281 327 ■ ■ i ■ ■ • 1 i ■ ■ ■ ■ । 1 1 1 ■ i ■ 1 ■ ' i ■ ■ ■ ■ i ■ ■ ' ■ i ■ ■ ■ ■ i 415 1 ■ ■ • i ■ 519 ' ■■ ■ 561■ 1 ' i 1 1 i AAMW WW m/z-> 50 100 150 200 _ 250 300__ 350 400 450__ 500 550 Abundance #30949: Mercaptoacetic acid, bis(trimethylsily!)- 73 38.60 38.80 39.00 39.20

N 147 m/z 354.95 25.90% 5000 221 45 . J, , J ,104, ... 193 / m/z~> 50 100 ' ' 150 200 250 300 350 400 450 500’550 38.60 38.80 39.00 39.20

1964.D GCMS0308.M Thu Mar 21 09:16:41 2002 Page 2

NYC-WTC_000010340

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NYC-WTC_000010340Source: NYC Law Department, mirrored locally

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