GCMS analysis results for sample AE04411, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2502\4411.D Vial: 17 Acq On : 26 Mar 2002 1:59 am Operator: Sample : gc/ms scan 2/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1-Monolinoleoylglycerol trimet Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

38.83 37.90 ug/1 2870670 Perylene-dl2 37.94

Hit# Of 5 Tentative ID MW MolForm CAS# Qual l 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 25 2 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 23 3 3 - Isopropoxy-1,Z 1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 12 4 Benzoic acid, , 5-bis (trimethylsilo 370 C16H3004Si 003618-20-0 10 Abundance Scan 3680 (38.830 min): 4411 .D 0 ~ Mt/ 73.0.0 100.00% 73 147 5000 221 281 355 429 38.40 38.60 38.80 39.00 39.20 m/z-> 45 ■ ■ i ‘ 50 117 ■ i ■ ‘ 100 150 +191- 200 [ 10 Ft"[ ■ 3271 251,, 250 300 350 11 TI i +— *401 400 450 500 550 m/z 147.00 66.42% Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 38.40 38.60 38.80 39.00 39.20 34 103 281 m/z 221.0, 49.59% 395....... 482.......... ■ i ' ' ■ ' i 1 ■ ■ ■ I ■ ‘ ' i ‘ ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance 2. ,1.6 .7- Hlep ne,) " not s ilo- y t 73

147 38.40 38.60 38.80 39.00 39.20 5000 267 • 355 429 45 207

■ ■ । 1 1 1 ■ i ■ ' • * i • ■ 1 ■ । ■ ■ ■ ■ । ■ i • ■ ■ ■ । * ■ • ■ । •1 ■ । ■ ■ • ■ । ■ i 1 ■ miz-> 50__ 100 150 200 250 300 350 400 450 500 __ 550 Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73 38.40 38.60 38.80 39.00 39.20 m/z 355.05 28.01% 5000 147

. 415. .519 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 38.40 38.60 38.80 39.00 39.20

4411.D GCMS0308.M Thu Mar 28 12:33:59 2002 Page 5

NYC-WTC_000011888