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GCMS analysis results for sample AE04411, April 2002

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Laboratory report documenting GCMS analysis of environmental sample AE04411 conducted on April 3, 2002.

NYC-WTC_000011877–000011892

Folder label: “GCMS X 2/28/02 A 3/26/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR25O2\4411.D Vial: 17 Acq On : 26 Mar 2002 1:59 am Operator: Sample : gc/ms scan 2/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

40.60 36.94 ug/1 2797530 Perylene-dl2 37.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3,6-Dioxa-2,4,5,7/tetrasilaoctane, 294 C10H3002Si 004342-25-0 23 2 2,6-Dimethyl-3,4 bis(trimethylsilyl 311 C15H29NO2Si 000000-00-0 12 3 Trisiloxane, 1, ,1,5, 5,5-hexamethyl 384 C12H3604Si5 003555-47-3 12 4 3-1sopropoxy-1, ,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 10 Abundance Scan 3873 (40.601 min): 4411.D (-) Z 73.00 100.00% 73 147 221 5000 281 355 429 40.20 40.40 40.60 40.80 41.00

m/z-> 45 1 96 117.. . +191,41251,444npor *****1* 1I——u—9002—80—0—8T 40 60 80 100120140160180200220240260280300320340360380400420440 327 m/z 146.95 70.43% Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 147 221

73 5000 40.20 40.40 40.60 40.80 41 loo 191 117 279 m/z 221.05 55.97% I I *1—“ Tppppmmomm m&-> 40 60 80 100120140160180200220240280280300320340360380400420440 Abundance ns 2 cdtmpmemtrg 73 221

40.20 40.40 40.60 40.80 41.00 5000 147 m/z 281.10 32.87% 178 45 296 TrrpTTTTTTTTpTTTpTTT^ m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 40.20 40.40 40.60 40.80 41.00 147 m/z 355.0 30.86% 5000 281 45 369 t......... 117..... , 207 249 Tp^TTT^TnrrriTTrrpTTT^ WnpaunnmmmmamWmmmmppun mlz~> 40 60 80 100120140160180200220240260280300320340360380400420440 40.20 40.40 40.60 40.80 41.00

4411.D GCMS0308.M Thu Mar 28 12:34:03 2002 Page 6

NYC-WTC_000011889

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NYC-WTC_000011889Source: NYC Law Department, mirrored locally

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