GCMS analysis results for sample AE04411, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2502\4411.D Vial: 17 Acq On : 26 Mar 2002 1:59 am Operator: Sample : gc/ms scan 2/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

42.80 25.79 ug/1 1952900 Perylene-d12 37.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O3Si6 038147-00-1 38 2 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 ) 071579-69-6 37 3 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 32 4 3-Trimethylsilyloxystearic acid, tr 444 C24H5203Si2/ 000000-00-0 10 Abundance Jean 4112 (42,796 min): 4411 .D (-) WWZ 73 147 221 5000 281 355 429 42.40 42.60 42.80 43.00 43.20 45 117. , 191 249, L 327. 401 1 ■ ■ i • ■ ‘ • i ■ • ' ■ i 1 ' ‘ ' i 1 ’ ■ ■ I ■ ‘ ‘ * i ' — ---------- m/z 147.00 72.25% m/z->__ 50__ 100__ 150__ 200 __ 250__ 300 350 400 450__ 500 550 Abundance #56714: 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73

147 5000

45 207 267 355 429 m/z 7 42.40 42.60 42.80 43.00 43.20

m/z-> 50 100 150 200 __ 250 300 350 400 450 500 550 Abundance ’ - jainopegon 73

42.40 42.60 42.80 43.00 43.20 5000 m/z 281.10 33.08%

"T 147

221 281 327 415 519 561 m/z-> 50 100 150 200 ' 250 300 350 400 ' 450 ' 500 ' 550 ‘ Abundance #41682:3,6-Dioxa-2,4.5,7-tetrasilaoctane. 2,2,4,4,5,5,7,7- 147 221 42.40 42.60 42.80 43.00 43.20 73 5000 191 117 279 ----------------- m/z-> 50 100 150 200 250 300 350 400 450 500 550 42.40 42.60 42.80 43.00 43.20

4411.D GCMS0308.M Thu Mar 28 12:34:08 2002 Page 7

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