NYC-WTC_000011877
Laboratory report documenting GCMS analysis of environmental sample AE04411 conducted on April 3, 2002.
Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Document / 15 pages
GCMS sample analysis results for AE01968, March 2002
Machine-extracted title · confidence 100%Laboratory report detailing the analytical results for sample AE01968 obtained via GCMS on March 22, 2002.
NYC-WTC_000010359–000010373Folder label: “GCMS X 1/27/02 A 2/26/02 - 3/5/02 3/20/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\MAR1902\1968.D Vial: 13 Acq On : 20 Mar 2002 4:46 pm Operator: Sample : gc/ms scan 3/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,1,1,5,7,7,7 -Heptamethyl-3,3- Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
38.86 7.08 ug/1 783392 Perylene-d12 37.97
Hit# of 5 Tentative ID MW MolForm CAS# Qual
l l,l,l,5,7,7,7-HeptameXhyl-3,3-bis(t 444 C13H40O5Si€ 038147-00-1 32 2 1,2-Benzenedicarboxylic acid, bis(t 310 C14H2204Si2 002078-22-0 14 3 3-Isopropoxy-l, 1,1,/,7,7-hexamethyl 576 C18H52©7Si7 071579-69-6 12 4 Trisiloxane, 1,1,1/5,5,5- hexamethyl 384 C12H3604Si 003555-47-3 12 Abundance 73 Scan 3684 (38.862 min): 1968.D (-) ' Ti T m/ 73.00 100.00% 147 221 5000 281 355 429 38.60 38.80 39'00 39'20 45 ■ 'i1 ’ 117.. j 191 — 249,j 1 3271. 401 L ■ ■ I ■ ■ 1 ■ i ' ‘ 1 1 i ---------- m/z 147.00 62.06% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance... #56714:1,1,1,5,7,7,7-Keptamethyl-3,3-bis(trimethylsiloxy)t 73
147 5000 267 TTnn 355 429 38.60 38.80 39.00 39.20 45 207 m/z 221.05 49.74% ' | ’ I’ m/z-> 50 100 150 ' 200 ' 250 ' 300 350 400 ' 450 500 550 Abundance 147 —PTTT 73 38.60 38.80 39.00 39.20 5000 m/z 281.05 27.57%
.. 7 45 295 119 193 221 m/z-> . 50 IPO 150 200 250 300 350 400 450 500 550 Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73 38.60 38.80 39.00 39.20
5000 147 221 281 327 415 519 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 38.60 38.80 39.00 39.20
1968.D GCMS0308.M Thu Mar 21 09:19:27 2002 Page 4
NYC-WTC_000010369
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