GCMS analysis results for sample AE04730, April 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2602\4730.D Vial.: 12 Acq On : 26 Mar 2002 8:36 pm Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

38.83 0.57 ug/1 43873 Perylene-dl2 37.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3 -Isopropoxy-1 A,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 28 2 Mercaptoaceti^ acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 17 3 Trisiloxane,/l,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 17 4 Indole, 2-benzoyl- 221 C15H11NO 001022-86-2 9 Abundance Scan 3680 (38.825 min): 4730.D (-) m/ z 737on ioo . 00% 7)3 147

221 5000 355 281 429 253,1 I I I 38.40 38.60 38.80 39.00 39.20 44 7^1 m/z I47T00’ ' 73.79*% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #605di 3-lsopropoxy-1,1.1,7.7,7-hexai'nethyl-3,5,5-trisCtrim 7)3

A/^fl ,A yI , I , //AM 5000 147 38.40 38.60 38.80 39.00 39.20 m/z 221.05 51.58% 221 281 327 415 519 561 m/z->______50 100 150 200 250 300 :350 400 450 500 550 Abundance #3();)40 Meio-Ptoacetic acid, b:4(tnn'cthy'siiy’!- 73 147 38.60 38.80 39.00 39^20 5000 m/z 355.0,5 34.98% 221 45 193 ■ , . 104

'm/z->50 100 __150__200___ 250 300 _ 350 400. 4M 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyf-3,3-bis[(trimet 73 147 38,4O_MJO_38^__39^_39;2O_

281 m/z 281.^ 26.38% 5000

36S 207 249 n-+ m/z-> 50 100 150 200 250 300 350 400 450 500 550 38.40 38.60 38.80 39.00 39.20

4730.D GCMS0308.M Thu Mar 28 16:31:58 2002 Page 4

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