NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\APR16O2\6635.D Vial : 8
Acq On : 16 Apr 2002 8:03 pm Operator:
Sample : gc/ms scan 3/22 Inst : 209
Mise : Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 7 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
40.50 2.89 ug/1 350725 Perylene-dl2 37.88
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy/l,1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 37
2 Trisiloxan^ 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 22
3 3,6-Dioxa-/, 4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 17
4 l,l,l,5,757,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 12
Abundance Scan 3862 (40.502 min): 6635. D (-) m/z 73.00 100.00%
73
147
221
5000
281 355
429
193
40.20 40.40 40.60 40.80
,, , , 253, [ ,327|
m/z 147.00 69.57%
Tl/Z~> . 50 100 150 200 250 300 350 400 450 500 550
Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim
7)3
253 .... ...... _
147 40.20 40.40 40.60 40.80
m/z 221.05 55773%
■n/z->
Abundance
5000
50
73
100 150 200 250 300 350 400 450
#74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(lrimet
147
500 550
A
40.20 40.40 40.60 40.80
m/z 281.00 32.66%
281
45 369 .................
I, 117 ■ , , ,2?^ 249.
■n/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #41682: 3,6-Dioxa-2.4,5,7-tetrasilaoctane, 2,2,4.4,5,5,7,7-
1 7 2’1 40.20 40,40 40.60 40.80
m/z 355.05 30.51%
73
253
191
117 279
, I , ,1 , , I , I, ) j , I
TlZz-> 50 100 150 200 250 300 350 400 450 500 550 40.20 40.40 40.60 40.80
6635.D GCMS0412.M Wed Apr 17 12:03:10 2002 Page 7
NYC-WTC_000060491
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