GCMS analysis results for sample AE05897, March 29 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2102\5897.D Vial: 25 Acq On : 22 Mar 2002 12:56 pm Operator: Sample : gc/ms scan 3/13 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

38.87 0.49 ug/1 88864 Perylene-dl2 37.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy71, 1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 37 2 3,6-Dioxa-2,A,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 37 3 1,1,1,5,7,7/7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 25 4 TrisiloxaneZ 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 12 Abundance ( ^n"3W(3O68niinr^ .. ’ "" m/ z 73 7'oo”. 100700% 73

147 221 5000 355 281 44 429 I ni/z-2>____ 50 100 150 ^7 1 -i-A 327, -'-I ' ' ............. 38.60 38.80 39.00 39.20 m/z 147’. 05 65.52%’ 200 250 300 350 400 450 500 550 Abundance #60503: 3-isopropoxy-1,1,1,7,7,7-liexamethyi-3,5,5-tris(trim 73

5000 147 38.60 38.80 39.00 39.20 221 281 . 327 m/z 221.05 56.82% 415 519 561 j I ' ' I ’m/z-> 50 100 150 200 250 300 :350 400I__ 450 500 550 Abundance 1632? 3.6-Dioxa-2 4,5 J-tctryslaodiarie? f; 4.4.5.5.7 147 221

73 _ 38.60 38.80 39.00 39.20 5000 m/z 355.0,5 33.58% 191 117 279

fn/z-> ... 50 ..... 100 __ 150___ 200 250 ___ 300 350 400 450 500 550 Abundance #56714: 1,1,1,5,7,7,7-Heptamethyi-3,3-bis(trimethylsiioxy)t . .. ...A, A....... 73 38.60 38.80 39.00 39.20

m/z-> 5000

Tl 50 100 147

207 J... I. I , 150 200 267

I, ,1 250 300 350 355

, I I............. 400 429

450 500 550 ZLXj 38.60 38.80 39.00 39.20

5897.D GCMS0308.M Mon Mar 25 14:27:25 2002 Page 3

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