GCMS results sample AE08215, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\APR1702\8215.D Vial: 26 Acq On : 18 Apr 2002 8:37 am Operator: Sample : gc/ms scan 4/8 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

37.31 0.51 ug/1 53740 Perylene-dl2 37.87 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy/l, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 32 2 3,6-Dioxa-2/4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 25 3 1,1,1,5,7, ,7-Heptamethyl-3;3-bis(t 444 C13H40O5Si6 038147-00-1 16 42,6-Dimeth 1-3,4-bis(trimethylsilyl 311 C15H29NO2Si2 000000-00-0 14 Abundance Scan 3514 (37.308 min): 8215.D (-) m/z 73.00 100.00% 73 147 221 5000 355 281 429 37.00 37.20 37.40 37.60 44 > ■ i ■ ■ ■I 1 ' ii 1 11 ' ■ 191 ).jaw 1327),.. | m/z 146.95 71.64% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

, AMA /Y 5000 147 37.00 37.20 37.40 37.60 m/z 221.05 51.24% • 1 I 1 271 21 327 ' > > I ■ ■ ■ > l - ■ ■ ■ 1 1 • ■ ■ l ■ ■ ■ ■ I ■ । 1 f l ■ ■ ■ • I 415 ■ ■ ■ 1 I । 1 > > T 1 ' 1 1 | ' । 519 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #41682:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 147 221 'I 1 1 1 1 1 1 1 ' 1 I 73 37.00 37.20 37.40 37.60 5000 m/ z 355.05 36.05% 191 117 279 .... L, i,, ■ ■ ।' ■ ■ ■ ।'''■' m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t i 1 ■ ■ ■ i1 ■ ' 1 i 73 37.00 37.20 37.40 37.60 m/z 281.10 29.25%

5000

n/z-> 1 45 I .. I, 'I 50 1 1 I I l > > I ‘ 100 147

150 207

200 267

250 300 355

350 400 429

■ i ■

450 i ■ ■ ■ ■

500 i ■ ■ ■ ■

550 i ■ ■ L 1 1 । ■ 1 1 1 । ■ ■ ' r । ' 1 । ' । 1 1 1 । । 37.00 37.20 37.40 37.60

8215.D GCMS0412.M Thu Apr 18 14:12:57 2002 Page 2

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