GCMS results sample AE08215, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\1\DATA\APR1702\8215.D Vial: 26 Acq On : 18 Apr 2002 8:37 am Operator: Sample : gc/ms scan 4/8 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Butyl hexadecanoate Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 29.96 0.29 ug/1 38112 Chrysene-dl2 33.64 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butyl hexa canoate 312 C20H40O2 000000-00-0 52 2 1-Undecene 2-methyl- 168 C12H24 018516-37-5 22 3 3-Undecene, 10-methyl- 168 C12H24 000000-00-0 22 4 Pentadecane, 8-methylene-________ 224 C16H32 055668-09-2 22 Abundance Scan 2714 (29.964 min): 8215.D (-) m/z 56.00 100.00% 55

5000 4 257 73 ...................... / . 129 239 Ti। 1 1 1 1 । 1 1 1 ' i ■ ■ ■ ■ । 1

m/z-> 1l,,27 101116/1, TPPTT 11.1 [ r. . i ] । rri । । । । । । 185 213 | __________ 312 TTud—u—un—————nnt । ■11 ‘ ।111 r ।111' । 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.60 29.80 30.00 30.20 m/ z 57.00 61.97% Abundance #44549: Butyl hexadecanoate 56

5000 258 TT AI1 Ii" 29.60 29.80 30.00 30.20 73 240 312 m/ Z 43.05 52.60% 129 101 . | | 157171195 214 .LI 1*199—009— i1 1' ■ r 1 ‘ I’’’ 'I' r 11 11 11 1 'i11 TT m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #68124:1-Undecene, 2-methyl- 56 A.............................. ............. 29.60 29.80 30.00 30.20 5000 m/ z 41.05 43.70%

42 83 I | 97 112 140 168 | i ~ I i" r | | i i 1 | i TTT100——TTtTTTTTOTgITT

m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance 56 #14691: 3-Undecene, 10-methyl- AA 1 । 1 r 1 ' । 1 ' 11 1 ' 1 1 ’ 1.......... 1 1 29.60 29.80 30.00 30.20 m/z 257.25 39.90%

5000 70 27 42 117 44 I 111125140 168 V ' • 1 ] ’ ' 1 T J I I T T | ' 1 1 ' | I I I I | 1 r r 1 | I r I I [I I I I [ I I I I | I I I I | I I I I | I f I I | I I I I [ ri I I | I I I I | .................. / ' । 1 1 1 1 । 1 1 ' ■ ' i ' 1 ■ ■ i ■ /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.60 29.80 30.00 30.20

8215.D GCMS0412.M Thu Apr 18 14:12:56 2002 Page 1

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