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GC/MS analysis results for sample AD22779, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22779 conducted on October 5, 2001, identifying unknown compounds.

NYC-WTC_000087694–000087716

Folder label: “GC/MS Scan 9/20/01

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Scanned page image, NYC-WTC_000087705
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT0201\22779.D Vial: 16 Acq On : 3 Oct 2001 4:48 am Operator: 2 09 GTkLOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Butyl hexadecanoate Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.54 1.26 ug/1 184782 Chrysene-dl2 33.15 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Butyl hexad^anoate 312 C2 0H40O2 000000-00-0 38 2 1-Hexene ^/5-methyl- 98 C7H14 003524-73-0 27 3 Cyclobujzane, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 4 Oxir^^e, 2,3-bis(1-methylethyl)-, t 128 C8H16O 054644-32-5 23 Abundance Scan 2668 (29.537 min); 22779. D (-) Tm/z 56.00 100.00% 53

5000 4 73 257 , , I , , 1 I I . , I Cl , . I

tVz-> 20 40 60 129 ,IJ. iUllAV I 143157171185i992p 80 100 120 140 160 180 200 220 240 260 280 300 XU 312 ' I'' '' I'' '' I 29.20 29.40 29.60 29.80 m/z 57700 447^9% Abundance #44549: Butyl hexadecanoate 53

5000 258 A 29.20 29.40 29.60 29.80 240 312 m/z43.05 36.43% 129 I I I 157171214 rThpTH-T-Yp-rV-^pnh-p-T-r-rpnn-Sp-iH^^ T Tife-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #63239:1-Hexene, S-methyl- 50 41 29.20 29.40 29.60 29.80 5000 m/z 41705 33.26% 70

n/z-> 20 11 40 Tp-n-rp- 60 98 '"T r' ' ' I ‘ ‘ ‘ I ' ' ' ' I ' ' ' ' I ' ‘ ' U ' * ' • I ‘ 80 100 120 140 160 180 200 220 240 260 280 300 ' I ' ‘ ' I ' ' ' ' I ' ' ' ' I

Abundance 53 #21985; Cyclobutane, 1,1-dimethyl-2-octyl- nA A' 29.20 29.40 29.60 29.80 m/z 55.00 27.17% 5000

27 70 A -..-LA.- 9,^ 111125140 168 196 ' ' I • -1 • I « • • « I •I I . I I I n I I » n I I I ' ' ' ' I p-r-rp-r-r-rp ,,, AA I'''' I'''' I Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

22779.D NP091101.M Thu Oct 04 14:21:17 2001 NYC-WTC_000087705

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NYC-WTC_000087705Source: NYC Law Department, mirrored locally

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