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GC/MS analysis results for sample AD22779, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22779 conducted on October 5, 2001, identifying unknown compounds.

NYC-WTC_000087694–000087716

Folder label: “GC/MS Scan 9/20/01

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Scanned page image, NYC-WTC_000087704
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File ; C:\HPCHEM\1\DATA\OCT0201\22779.D Vial: 16 Acq On 3 Oct 2001 4:48 am Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 11.64 0.52 ug/1 65499 1,4-Dichlorobenzene-d4 11.78 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichlprobenzene-d4 150 C6C12D4 003855-82-1 50 2 Benzene/T,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 12 3 2-MeWiyl-6-nitroaniline 152 C7H8N2O2i 000570-24-1 10 4 Ben^i^dehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 Abundance Scan 719 (11.644 min): 22779.D (-) Tm/z 149.90 100.00% 1!i0

5000 115 52 78 T 11.40 11.60 11.80 12.00 ..........- I m/z 151.90 . 65.06% ........... ...................... ' I'''' I Ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1.4-Dichlorobenzene-d4 It®

115 7 5000 1'^' ' I 78' 11.40 11.60 11.80 12.00 52 m/z 115.00 . 31.38% 35 .. I ‘' I n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- lilO /

115 11.40 11.60 11.80 12.00 5000 52 78 Wz 77.95 . 17.38%

87

Tife-> 20 30 35 I 40 50 ' I ' '’ ' I ' 60 70 I I ' ' ' ' I'' ' ' I 80 90 A 100 110 120 130 140 150 160 4+^ ^bundance #66883: 2-Methyl-6-nitroaniline 77 152 11.40 11.60 11.80 12.00 Wz 52.00 . 14.27%

5000 106 52

I Tife-> 20 30

30 40 I T-p-n-r-j-r 50 60 70 80 90 94

100 110 120 130 140 150 160 11.40 11.60 11.80 12.00

22779.D NP091101.M Thu Oct 04 14:21:15 2001 Paae 4 NYC-WTC_000087704

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NYC-WTC_000087704Source: NYC Law Department, mirrored locally

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