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GC/MS analysis results for sample AD23262, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23262 conducted on October 12, 2001.

NYC-WTC_000088115–000088179

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088143
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OGT0901\23263 .D Vial: 9 Acq On 9 Oct 2001 9:11 pm Operator: 209 GALOS Sample g c/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 11.62 0.57 ug/1 131279 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichlo^benzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-ly^,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 32 3 2-Methy^-nitroaniline 152 C7H8N2O2i 000570-24-1 10 4 4-Aminok2-chlorobenzonitrile 152 C7H5C1N2 020925-27-3 10 Abundance Scan 717(11.624 min): 23263.D (-) m/z 149.90 100.00% 1'10

5000 115 52 78 H ' ' ' I ' ' ' ' r ' ' • I '' 11.20 11,40 11.60 11.80 12.00 m/z 151.90 65.87% TiZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 ' ' I ' ' 78 11.20 11.40 11.60 11.80 12.00 52 m/z 115.00 36.84% 35 I' ' '' I tVz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1$0 \ . , , , y , . , , , 115 11.20 11.40 11.60 11.80 12.00 Esa 52 78 "mTz 78.05 19.84%

35 87 1 I .. ' I ' ‘ ' I ' ' I''' ‘ I' tVz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66883: 2-Mefhyl-6-nitroaniline 77 . 152 11.20 11.40 11.60 11.80 12.00 ■m/z 52.00 16.08%

5000 106 52 30 94 ' I ' ' ' ' 1 ' ' ' ' I ' ' ...... ' ' I' Tl/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

23263.D NP091101.M Thu Oct 11 10:50:31 2001 Page 2

NYC-WTC_000088143

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NYC-WTC_000088143Source: NYC Law Department, mirrored locally

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