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GC/MS analysis results for sample AD23262, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23262 conducted on October 12, 2001.

NYC-WTC_000088115–000088179

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088144
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0901\23263.D Vial: 9 Acq On : 9 Oct 2001 9:11 pm Operator: 2 09 GTUjOS Sample : g c/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentanecarboxylic acid, 2 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

29.51 1.99 ug/1 425725 Chrysene-dl2 33.13

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 Cyclopent^ecarboxylic acid, 2-amin 129 C6H11NO2; 037910-65-9 38 2 Oxirane/ 2,3-bis(1-methylethyl)-, t 128 C8H16O 054644-32-5 32 3 Cyclobytane, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 4 1-Hex/ne, 2-methyl-_____________ 98 C7H14 006094-02-6 27 Abundance / Scan 2665 (29.507 min): 23263.D (-) m/z 56.00 100.00% 53

5000 4- 73 . .... , , / p , I . , , . I I 129 257 29.20 29.40 29,60 29.80 ,I 312 ■p m/z 57.00 45737% 7i/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5218: Cyclopentanecarboxylic acid, 2-amino-, cis- 5^

5000 29.20 29.40 29.60 29.80 m/z 43.05 36.15% 30 100 129 ,1 J 54 ■■[■■■•r-rJ .................... i ' ' ' ' I ' ' ' ' I' '' ' I TT/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 ^bundance #5067: Oxirane, 2,3-bis(1 -methylethyl)-, trans- 53 41 29.20 29.40 29.60 29.80 5000 m/z 41.05 34.79% li 73

113128.......... .............. ... n/z-> Abundance 20 40

53 60 80 100 120 140 160 180 200 220 240 260 280 300 #21985: Cyclobutane, 1,1 -dimethyl-2-octyl- ' ,1a T ' ' ' 'I ' 29.20 29,40 29,60 29.80 m7z 73.00 30.11% 5000

■n/z-> 27

20 I 40 w 60 70

80 7 111125140 168 196 '' r ' '' I' ''' I ‘' I' I' ' r ' ‘ ' I I ' ' ' 'I ' '•' I' 100 120 140 160 180 200 220 240 260'280 300 'I ' I ' ' ‘ I , .7.1, . 29.20 29.40 29.60 29.80 , , , , ,,

23263.D NP091101.M Thu Oct 11 10:50:33 2001 Page 3

NYC-WTC_000088144

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NYC-WTC_000088144Source: NYC Law Department, mirrored locally

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