GCMS results log, sample AD27007, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 601\27007.D Vial: 22 Acq On 7 Dec 2001 5:16 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentanecarboxylic acid, 2 Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

29.59 0.72 ng/uL 211059 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentanecarboxylic acid, 2-amin 129 C6H11NO2 040482-05-1 38 2 Cyclopent ecarboxylic acid, 2-amin 129 C6H11NO2 037910-65-9 38 3 Oxirane,/ ,3-bis(1-methylethyl)-, t 128 C8H160 054644-32-5 37 4 1-Hexene, 2-methyl- 98 C7H14 006094-02-6 35 'Abundance Scan 2699 (29.592 min): 27007.D (-) m/ z 56.10 100.00% 55

5000-

L 43 73 "T 230 257 i • • ■ 'I 1 ' 1185,8711912 157 — , 185.............. AL 29.20 29.40 29.60 29.80 30.00 m/z 57.10 44.26% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #5212: Cyclopentanecarboxylic acid, 2-amino-, trans­ 56

5000 - TF / MA_ 29.20 29.40 29.60 29.80 30.00 m/z 43.10 42.31% 30 69 82 100 129 .1 42 i ■ • ■ ■ i ■ ■ >ll 1

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #5218: Cyclopentanecarboxylic acid, 2-amino-. cis- 56 I / A 29.20 29.40 29.60 29.80 30.00 5000 - m/z 41.10 41.28%

30 • 69 82 100 129 42 m/z-> Abundance 20 i ' ' ■ ' i ' 40 ’

56 60 t

80 100 120 140 160 180 200 #5067: Oxirane, 2,3-bis(1-methylethyl)-, trans- 220 240 260 ' I ■ ' ■ ' I ' ' W 29.20 29.40 29.60 29.80 30.00 41 m/z 55.10 28.26% 5000 73

m/z-> 20 i '' ■ ' i

40 ■ ■

60 I 80 100 113 128 120 140 160 180 200 220 240 260 T —A— 29.20 29.40 29.60 29.80 30.00 T"T

27007.D NP112701.M Tue Dec 11 14:56:49 2001 Page 3

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