GCMS results log, sample AD27007, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 601\27007.D Vial: 22 Acq On 7 Dec 2001 5:16 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1-Hexene, 2-methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

31.72 0.46 ng/uL 135527 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Hexene, 2/methyl- 98 C7H14 006094-02-6 27 2 Cyclopentanecarboxylic acid, 2-amin 129 C6H11NO2 040482-05-1 25 3 2-Chloro-2-methylnonane 176 C10H21C1 004325-50-2 25 4 2-Methy^Z-N-l-tridecene 196 C14H28 018094-01-4 25 Abundance Scan 2931 (31.719 min): 27007.D (-) m/z 56. 0 100.00% 53

5000- 43 73 - . 129 31.40 31.60 31.80 32.00

miz-> I ' ' ' ' 1 1 1 20 40 60 L 85.971174 80 100 120 140 160 185 180 200 220 240 267 285 260 280 m/z 57.10 53.13% Abundance #1354: 1-Hexene, 2-methyl- i 56 41 5000 PT ' —Ir i 31.40 31.60 31.80 32.00 27 m/z 43.10 46.88% 70 1 1 83 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #5212: Cyclopentanecarboxylic acid. 2-amino-. trans- 1

5000- 56

m/z . A 31.40 31.60 31.80 32.00 41.10 fIT 40.68%

i 30 42 69 82 100 129 ! • ‘ TITEEI-T m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #16689: 2-Chloro-2-methylnonane ‘II I i 56 ■ 31.40 3i60 31.80 32.00 i 69 m/z 55.10 39.11%

5000

m/z-> 35 i ' ■ ' ' i 1 1 20 40 60 1L1 97112125.140 80 100 120 140 160 180 200 220 240 260 280 ■ ■ i ' ■ ■ ■ 31.40 31.60 31.80 32.00 i ■ -----

27007 .D NP112701 .M Tue Dec 11 14:56:54 2001 Page 4

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