GCMS results log, sample AD26833, Dec 11 2001

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Laboratory report for GCMS analysis of sample AD26833 completed on December 11, 2001, showing surrogate recovery data.

NYC-WTC_000032286–000032307

Folder label: “GCMS X 11/8/01 A 12/7/01”

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NYC 9/11 Public Portal Document

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Data File C:\HPCHEM\1\DATA\DEC0601\26833 . D Vial: 33 Acq On 7 Dec 2001 4:14 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentanecarboxylic acid, 2 Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

29.58 5.96 ng/uL 1980120 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentaneca rboxylic acid, 2-amin 129 C6H11NO2 040482-05-1 43 2 1-Hexene, 2- thyl- 98 C7H14 006094-02-6 38 3 1-Undecene, /2-methyl- 168 C12H24 018516-37-5 32 4 Butyl hex. .ecanoate 312 C20H40O2 000000-00-0 32 Abundance Scan 2698 (29.584 min): 26833.D(-) m/z 56.10 100.00% 55

5000 41 .............................................................. 73 257 I 27,101115122143157171 185199213,.. 232 312 TWWTPPTTTTTT 29.20 29.40 29.60 29.80 30.00 m/z 57.10 47.53% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5212: Cyclopentanecarboxylic acid, 2-amino-, trans- 56

5000 Td LU__ 29.20 29.40 29.60 29.80 30.00 m/ z 41.10 37.84% i 30 100 129 |m/z-> | 20 4 —40 £60 79 8084 100 ‘I I"IE ______ ‘ I 11-TTI-IETTVTCITECTTTTTTIT‘T‘II 120 140 160 180 200 220 240 260 280 300 i' ■ ' ' i'111 I

'Abundance #63261: i-Hexene, 2-methyl- 56

29.20 29.40 29.60 29.80 30.00 41 5000 m/ z 43.10 37.56% 27 70 98 m/z-> Abundance > ■ i• ■ • • i • ■ ■ • i • ■ ' • i ■ 20 40 60

56 80 TIT ।' i ■' ■' । ■ ■ ■ ■ ।। ■ 11 ■' ■ । 100 120 140 160 180 200 220 240 260 280 300 #14760: 1-Undecene, 2-methyl- ।'1111' ■ । ■ ■' ■ ।

TT LUA 29.20 29.40 29.60 29.80 30.00 m/ Z 55.1,0 29.72% 5000-

70 . TTT 42 I Tu 44,98,112, 140 168 IIPupumBWWmoor TWu—T .......... I N A..... m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80 30.00

26833.D NP112701.M Tue Dec 11 14:46:34 2001 Page 3

NYC-WTC_000032296

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NYC-WTC_000032427

Laboratory report for GCMS analysis of sample AD26987 completed on December 11, 2001.

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