GCMS results log, sample AD27008, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C : \HPCHEM\1\DATA\DEC0601\27008.D Vial: 21 Acq On 7 Dec 2001 4:21 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentanecarboxylic acid, 2 Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

29.59 0.47 ng/uL 149718 Chrysene-dl2 33.19

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentanecarboxylic acid, 2-amin 129 C6H11NO2 040482-05-1 43 2 1-Hexene, 2-Methyl- 98 C7H14 006094-02-6 35 3 1-Hexene, 2-methyl- 98 C7H14 006094-02-6 35 4 Cyclopentanone, 2,2-dimethyl -_______ 112 C7H120 004541-32-6 25 Abundance 3 Scan 2699 (29.590 min): 27008.D (-) m/z 56.10 100.00% 56

5000- 43 73 116 129 239 257 4,785 , 101 29.20 29.40 29.60 29.80 30.00 Li 4. .. . ............... .. । —___ \__ • ■ ■ l 1 ■ • ■ p m/z 57.10 51.39% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #5212: Cyclopentanecarboxylic acid, 2-amino-, trans- 56

5000 - ................................. 29.20 29.40 29.60 29.80 30.00

30 m/z 43.10 43.62% 42 100 129 69 82 .1 ' i 1 ■ ■ 1 ...... . m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #1354: 1-Hexene, 2-methyl- i 56 TI , AA... 1 II 41 29.20 29.40 29.60 29.80 30.00 5000 m/z 41.10 40.08% 27 70 83 98 • i • ■ • ■ । ■ ■ 1 i ■ O _ _ m/z-> Abundance 20 40

56 60 80 100 120 140 160 180 #63261: 1-Hexene, 2-methyl- 200 220 240 260 .. — A A 29.20 29.40 29.60 29.80 30.00 m/z 55.10 27.53% 41 5000- 27

15 70 1 98 — ' i ' ' ' ' i ' ' ' I m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 29.20 29.40 29.60 29.80 30.00

27008.D NP112701.M Tue Dec 11 14:58:02 2001 Page 3

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