GCMS results log, sample AD27009, Dec 11 2001

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\27009.D Vial: 28 Acq On 7 Dec 2001 11:38 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentanecarboxylic acid, 2 Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

29.59 4.27 ng/uL 1896880 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentane carboxylic acid, 2-amin 129 C6H11N02 037910-65-9 43 2 Cyclopentane carboxylic acid, 2-amin 129 C6H11NO2 040482-05-1 43 3 Cyclobutane, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 38 4 1-Hexene, 2-methyl-___________________ 98 C7H14 006094-02-6 38 Abundance Scan 2699 (29.591 min): 27009.D (-) m/ z 56.10 100.00% 56

5000 43 73 257 / 101 11611143 157171 185 199213 239 29.20 29.40 29.60 29.80 30.00

m/z-> I 1 1 1 1T 20 40 60 Al————— 80 100 120 140 160 180 200 220 240 260 280 300 1 — T PBII—uBp——r 312 m/z 57.10 48.09% Abundance #5218: Cyclopentanecarboxylic acid, 2-amino-, cis- 56

5000 I 29.20 29.40 29.60 29.80 30.00 m/z 43.10 40.18% 30 69 82 100 129 ji____ 1 i ■1 • ■ i ■''' i ■ ■1" । ■ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5212: Cyclopentanecarboxylic acid. 2-amino-. trans- 56 T A 29.20 29.40 29.60 29.80 30.00 5000 m/z 41.10 36.58%

30 69 82 100 129 I I TET ।, । "‘ "1 । ■ ■ • ■ । ■ ■ i ■ • ■ ■ । > i' ■' ■ i ' ■ ' ■ i ■ ■ ' ■ i ■ ' ■ ■ i ' ' ' ' i ■ ■' • i' ' ' ' i • • ' • i m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 'Abundance #21985: Cyclobutane, 1,1-dimethyl-2-octyl- "I ) "I 56 29.20 29.40 29.60 29.80 30.00 m/ Z 55.10 30.15% 5000

I 27 70 83 97 111 125 140 168 196 _____________ / kJ IIt‘11"" TTTTTTT , । TITTTTTTTTT i ■ ■ ■ ■ i ■ ■' ■ i' ■'' i' ■ ■ ■ r ■'' I • I ' 1 ’ 1 I • ' ' 1 I ' ' TT-f-r-r m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80 30.00

27009.D NP112701.M Tue Dec 11 14:59:26 2001 Page 3

NYC-WTC_000032543