GCMS results log, sample AD27009, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0601\27009.D Vial: 28 Acq On 7 Dec 2001 11:38 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Eicosane Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

2 9.70 0.73 ng/uL 323601 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2 3 4 Eicosane Tricosane Pentadecane Heptadecane, Abundance 282 324 212 8-methyl-______________ 254 Scan 2711 (29.701 min): 27009.D (-) C20H42 C23H48 C15H32 C18H38 m/ z 000112-95-8 000638-67-5 000629-62-9 013287-23-5 72 57.10 100. 00% (3) 80

57 43 71 5000 85

99 113 127141 155 A 29.40 29.60 29.80 30.00

m/z-> I 1 1 T‘ 1 1 40 60 1 1 1y 80 + I,I , ‘I‘ Trr’II T’EEII’r 1 I j f 1 ! I ( 100 120 140 160 180 200 220 240 260 280 300 320 m/ z 43, . 10 71.98% Abundance #72323: Eicosane 43 57

5000 - 71 85 .. LU.... 29.40 29.60 29.80 30.00 m/z 71 .05 58.81% ii 99 113 1 27 141 TTqpmnT-rTn-ryrrTTTT-rTTTT-rT-rp-rT-^^ 282 !>>>>! ■ i ■ 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #73318: Tricosane 43 57

71 29.40 29.60 29.80 30.00 5000- 85 m/z 85.05 48.30%

89 113 127 141 183197211225 296 324 ; — -P T > 1111 PTpr । । । । ■ । > i ii |i.t > । । > > t । । 1' r 1'1 i1 1 m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 — Abundance #70278: Pentadecane A ■' i ■ ■ ■ ■ i ■ ■ • ■ । 43 57 29.40 29.60 29.80 30.00 m/z 41 . 10 31.89% 71 5000- 85

99 113127141 155169 212 TIT -p-T TTIPTmpmm II- —PPPP m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 29.40 29.60 29.80 30.00

27009.D NP112701.M Tue Dec 11 14:59:28 2001 Page 4

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