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GCMS results log, sample AD27008, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD27008 completed on December 11, 2001.

NYC-WTC_000032520–000032533

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\27008. D Vial: 21 Acq On 7 Dec 2001 4:21 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Eicosane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

33.74 0.41 ng/uL 129566 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8/86 2 Eicosane, 10-methyl- 296 C21H44 054833-23-7 86 3 Nonadecane 268 C19H40 000629-92-5 86 4 Tricosane 324 C23H48 000638-67-5 86 Abundance Scan 3152 (33.744 min): 27008.D (-) m/z 57.10 100.00 57 43 71 5000 85 A 1"1 I _______TT 99 113 226 33.40 33.60 33.80 34.00 , Il __1 1 —............ 207 | m/ z ( 60.87% i1' TT" m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #72326: Eicosane 57 43 71 5000 IT 85 33.40 33.60 33.80 34.00

99 m/ z 4 3.10 59.97% ■ ■ । ■ — 11 ■ ■ • ■ । ■ 1,113 127 141 155 .............................. . ..,. m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42197: Eicosane. 10-meihyl- 43 57 -AA—— p-rrrj-rrrr-p-rrrp 71 33.40 33.60 33.80 34.00 5000 85 m/z 85.1 38.62% 99 •• 113 I • ■ i ■ ■ ■ 1 I • 141 154 168 268 296 m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #37469: Nonadecane ■ ■ l • • • ■ l ■ • ■ ■ i ■ ■ ■ ■ i ' 57 33.40 33.60 33.80 34.00 43 m/z 41.10 71 32.31% 85 5000

m/z—> ■ ■ i ■ ■ 40 60 IL 1 i ' ■ 1 ■ i 1 80 2.113,127— 100 120 140 160 183 197 180 200 220 240 260 268 280 300 _A... TKEEE-TLU I ( ] . 33.40 33.60 33.80 34.00

27008.D NP112701.M Tue Dec 11 14:58:10 2001 Page 5

NYC-WTC_000032532

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NYC-WTC_000032532Source: NYC Law Department, mirrored locally

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