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Document / 27 pages

GCMS results log, sample AD26985, Dec 11 2001

Machine-extracted title · confidence 95%

Laboratory report for GCMS analysis of sample AD26985 completed on December 11, 2001, showing surrogate recovery.

NYC-WTC_000032400–000032426

Folder label: “GCMS X 11/8/01 A 12/7/01

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Scanned page image, NYC-WTC_000032418
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26986.D Vial: 32 Acq On 7 Dec 2001 3:19 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Eicosane Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

29.70 0.46 ng/uL 167775 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 teO 2 Nonadecane 268 C19H40 000629-92-5 87 3 Tetracosane 338 C24H50 000646-31-1 86 4 Eicosane 282 C20H42 000112-95-8 80 Abundance Scan 2711 (29.698 min): 26986.D (-) m/z 57.10 100.00% 7

43 71 5000 85 » < I ‘ ' 1 - I

3 98113127............ I | T I . I p l i • | ! ! , I ! . ! I I | I I • • | • I • I | 29.40 29.60 29.80 30.00 m/ z 43 . 10 64.17% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #72323: Eicosane 43 57 71 5000- AT—— 85 29.40 29.60 29.80 30.00 m/ z 71.05 55.64% ! 1l99 113127141 TII—000r '1 ■ i''' ■ i • ■1 ' i ■' ■ ' I' ' '' i I ‘ ' I '' •' i'' ’' I' ‘* I 282 ■ i ■ • • ■ i • • ■ ■ I Tr m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #37469: Nonadecane 57 43 71 —— I l » ■ 29.40 29.60 29.80 30.00 85 5000 m/ z 85.05 40.97%

" 113127 183197 268 ‘‘0"E‘1111EET r r TTTTTTT r i r | r i > i | TTTTT y ■ i ■ ■ • ■ i • ■ ■ • i ■ ■ ■ > i

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane -4 43 57 29.40 29.60 29.80 30.00 71 m/ z 41 . 05 22.66% 5000- 85

99 1 113127 155169183197 294 338 . | , U I | I ‘t . | T TTTumuuui r '' ■ r '' ‘ i '''' r ' ■ ■ i i' ■ ■ ' i ■ T-r-| —9 1 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 29.40 29.60 29.80 30.00

26986.D NP112701.M Tue Dec 11 14:51:37 2001 Page 10

NYC-WTC_000032418

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NYC-WTC_000032418Source: NYC Law Department, mirrored locally

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