GCMS analysis results for sample AD26626, Dec 10 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26626.D Vial: 3 Acq On 6 Dec 2001 11:59 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Eicosane Concentration Rank 20

R.T. EstConc Area Relative to ISTD R.T.

29.70 0.41 ng/uL 93226 Chrysene-dl2 33.18

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 64 2 Hexacosane 366 C26H54 000630-01-3 56 3 Eicosane 282 C20H42 000112-95-8 56 4 Pentadecane 212 C15H32 000629-62-9 56 Abundance Scan 2711 (29.699 min): 26626.D (-) m/ z 57.10 100.00% 57

5000 4 85

. 113 A..... 29.40 29.60 29.80 30.00 l T‘‘t — m/ z 72.35% miz-> 40 60 ■ ■ i ■ I •''b 11''' I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 I 1‘ '1 | ' | 71.05 Abundance #72324: Eicosane 43

71 5000 I1 A 1L 29.40 29.60 29.80 30.00 m/z 43.10 66.20% 99 I | _ I J 141 169 197 254 282 ‘I’ 1 p . TTTTrr l '.... p 11 ■ ■ ■ i ■ ■'' i ■' ■ ■ i ■ ■ ■ • i ■ ■'' i

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73942. Hexacosane 57 AA 29.40 29.60 29.80 30.00 5000 m/z 85.05 43.76% ■ 85

| i 7 - i • I ■ •' TTT " 113 . •1 • ■ । 197 225 253 281 338 366 I' ■'1 11''1 1 1' 1 ' i 11 i r 1 ■11' 1 r 1 i'' ’1 i ' 1'' i 1' ’1 i1'1 1 r 1'' i''' 'm/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance 57 #72323: Eicosane A 29.40 29.60 29.80 30.00 m/z 41 . 05 28.15% 5000- 85

42 ,1 113 . 141 282 / •' I'1 - 11.. i. । i p i । it i. । 1! TTTTT r ] ।11.... 11»TTT 111 < । < । • 11 P ।«> । < t "I vi m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 29.40 29.60 29.80 30.00

26626 .D NP112701.M Fri Dec 07 14:50:22 2001 Page 13

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