GCMS results log, sample AD27009, Dec 11 2001

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Data File C:\HPCHEM\l\DATA\DEC0601\27009.D Vial: 28 Acq On 7 Dec 2001 11:38 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Eicosane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

34.67 1.58 ng/uL 702774 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS# %)

1 Eicosane 282 C20H42 000112-95-887 / 2 Pentacosane 352 C25H52 000629-99-2 87 3 Octadecane 254 C18H38 000593-45-3 86 4 Heptacosane 380 C27H56 000593-49-7 86 Abundance Scan 3253 (34.671 min): 27009.D (-) m/z 57. ,0 100.00% 57 43 71 5000 85

99

miz-> — 40 1—4 . l . 113 127 141 154 ...................................... (60 80 100 120 140 160 180 200 220 240 260 280 m/z 34.40 34.60 34.80 35.00 43. 0 67.08% Abundance #72323: Eicosane 43 57 71 5000 r TiLT 85 34.40 34.60 34.80 35.00 m/z 62.60% 11 99 113 127 141 282 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #73718: Pentacosane 43 57 TIPTIT ' ' ’ I ' • ' 1 I 1 ' Tef f ■ ' 71 34.40 34.60 34.80 35.00 5000 85 m/z 85.05 41.45%

1 ■ 99 113 127 141 155 169 183 197 211 225 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #71560: Octadecane 41 IET 43 57 34.40 34.60 34.80 35.00 m/ Z 55.10 29.23% 71 5000 85

99 1 ■ i ' — 113 127 141 169 183 197 210 254 ' 1 i ■ ■ ■ ! i ' ' 1.4AAP-4-r ■ • i • ■ M AA, m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 34.40 34.60 34.80 35.00

27009 .D NP112701.M Tue Dec 11 14:59:41 2001 Page 10

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