GCMS results log, sample AD27009, Dec 11 2001

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Data File C:\HPCHEM\1\DATA\DEC0 601\27009.D Vial: 28 Acq On 7 Dec 2001 11:38 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Hexadecane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

33.74 2.29 ng/uL 1016130 Chrysene-dl2 33.19

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadecane 226 C16H34 000544-76-3 91 2 Hexadecane 226 C16H34 000544-76-3 91 3 Pentacosane 352 C25H52 000629-99-2 91) 4 Heptacosane 380 C27H56 000593-49-7 90 Abundance Scan 3152 (33.745 min): 27009.D (-) m/z 57.10 100.00% 57 43 71 5000 85 ) __ 99 ... 33.40 33.60 33.80 34.00 : .... — IT TU ll 113 127 141 . 155 169 183 .... . m/ z 43.10 71.72% m/z-> 20 40 ।60 80 100 120 140 160 180 200 220 Abundance #70788: Hexadecane 57 43 71

i

m/z-> 5000-

। --T —II :20 40 60 80 85

99 113 127 141 155 169 183 100 120 140 160 180 200 226 220 7! J -I , PPP i । |'i 33.40 33.60 33.80 34.00 m/ Z 60.53%

Abundance #70787: Hexadecane 43 57 T 71 33.40 33.60 33.80 34.00 5000- m/ Z 85.05 40.63% 85

' 27 ; 1 99 113 127 141 155 226 ■ I ' ■ m/z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #73718: Pentacosane 433 57 33.40 33.60 33.80 34.00 m/z 55.10 25.87% I 71 5000 85

.... — l80 99 113 127 141 155 169 183 197 211 225 P -PPPPP I ' ' ' 1 I ' m/z-> 20 40 60 100 120 140 160 180 200 220 33.40 33.60 33.80 34.00

27009.D NP112701.M Tue Dec 11 14:59:39 2001 Page 9

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