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GCMS results log, sample AD26985, Dec 11 2001

Machine-extracted title · confidence 95%

Laboratory report for GCMS analysis of sample AD26985 completed on December 11, 2001, showing surrogate recovery.

NYC-WTC_000032400–000032426

Folder label: “GCMS X 11/8/01 A 12/7/01

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Scanned page image, NYC-WTC_000032423
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26986.D Vial: 32 Acq On 7 Dec 2001 3:19 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Heptadecane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

33.75 1.28 ng/uL 463128 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS#

1 Heptadecane 2 Heptadecane 240 C17H36 240 C17H36 000629-78-7 90 000629-78-7 (93/ T} 3 Hexadecane 226 C16H34 000544-76-3 90 4 Eicosane 282 C20H42 ____ 000112-95-8 86 Abundance Scan 3153 (33.752 min): 26986.D (-) m/ z 57.10 100.00% 57

43 71 5000 85

99 113

m/z-> rT—I4 40 60 +80 — —L, 127 141 100 120 140 160 169 180 200 207 220 226 240 240 33.40 33.60 33.80 34.00 m/ Z 43. 0 64.76% Abundance #71191: Heptadecane 43 57 i 71 5000 IT 85 33.40 33.60 33.80 34.00 1 m/z 71.05 59.80% li Td ii +aor 99 113 127 141 ............. 240 m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #71194; Heptadecane 43 57 ----- 71 33.40 33.60 33.80 34.00 5000 m/ z 85.05 36.56% 85

99 113 127 141 155 169 1 83 212 240 m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #70790: Hexadecane — 43 57 33.40 33.60 33.80 34.00 m/ Z 27.46% 71 5000 85

1 ' 1 1 — . 113127 141 155 169 182 2'6 A A ' ' I ■ • ' • l ■ .................... ' I -A-r 'm/; 40 60 80 10G 120 140 160 180 200 220 240 33.40 33.60 33.80 34.00

26986.D NP112701.M Tue Dec 11 14:51:47 2001 Page 15

NYC-WTC_000032423

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NYC-WTC_000032423Source: NYC Law Department, mirrored locally

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