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GCMS results log, sample AD26845, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD26845 completed on December 11, 2001, indicating unknown compounds.

NYC-WTC_000032308–000032320

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26845.D Vial: 29 Acq On 7 Dec 2001 12:35 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Hexadecane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

33.75 0.47 ng/uL 182580 Chrysene-dl2 33.19 .

Hit# of 5 Tentative ID MW MolForm CAS# Q

1 Hexadecane 226 C16H34 000544-76-3 90 2 Heptadecane 240 C17H36 000629-78-7 90 3 Heptadecane 240 C17H36 000629-78-7 90/ 4 Hexatriacontane ________ _ __________507 C36H74 000630-06-8 87 Abundance Scan 3153 (33.753 min): 26845.D (-) m/z 57.10 100.00% 57

43 71 5000 85 ...... 33.40 33.60 33.80 34.00 I I T1 2 113 127 > I .... . .......... ...... 226 240 m/z 43. ,0 62.26% m/z-> :20 I ’ 1 I 1 40 60 g0 100 120 140 160 #70786: Hexadecane 180 200 220 240 Abundance i 43i 57

71 5000 - 85 A.... 4 4 33.40 33.60 33.80 34.00 TT

27 m/z 71.05 56.58% , i 1 1 r'_i j I 99 113 127 141 155 169 183 ......... 226..... m/z-2 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #71193: Heptadecane I 57 —A 71 33.40 33.60 33.80 34.00 5000 - 85 m/z 85.15 37.64%

99 113 127 141 -155 169 210 240 m/z->20 40 60 80 100 120 140 160 180 200 220 240 Abundancei #71192: Heptadecane __ 1 1 1 ’ - 43 57 33.40 33.60 33.80 34.00 m/z 55.10 25.37% 71 5000- 85

miz-> 20 40 I —l — 99 113 127 60 80 100 120 140 155 169 183 197 160 180 200 220 240 240 —P —UM—..... 33.40 33.60 33.80 34.00

26845.D NP112701.M Tue Dec 11 14:47:29 2001 Page 4

NYC-WTC_000032319

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NYC-WTC_000032319Source: NYC Law Department, mirrored locally

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