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GCMS analysis results for sample AD26626, Dec 10 2001

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Laboratory report documenting GCMS analysis of sample AD26626 identifying unknown compounds on December 10, 2001.

NYC-WTC_000031940–000031967

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26626.D Vial: 3 Acq On 6 Dec 2001 11:59 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 18 Hexadecane Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

33.75 1.03 ng/uL 232841 Chrysene-dl2 33.18

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadecane 226 C16H34 000544-76-3 2 Hexadecane 226 C16H34 000544-76-3 93 3 Hexadecane 226 C16H34 000544-76-3 92 4 Eicosane, 10-methyl- 296 C21H44 054833-23-7 91 Abundance Scan 3153 (33.752 min): 26626.D (-) m/z 57. .0 100.00% 57 43 71 5000 - 85 Tif 99 113 127 141 33.40 33.60 33.80 34.00

m/z-> 11" । 11111 + ------- I' " ■ r ■ " I" "T'" 'T TTTBI‘‘I rt . , 40 50 60 70 80 90 100 110 120130140 150 160 170 180 190 200 210 220 230 207 2?6 m/z 43.10 73.57% Abundance #70790: Hexadecane 43 57

71 5000 ■ ■ i ' ■ 1 ' i ' ■ TIII 85 33.40 33.60 33.80 34.00 m/ Z 71.05 58.78% I 99 113 127 141 155 169 182 226 I " ' ' f" " I ।ii•I।ii•i।iii>।ii । > t i a |'t i i i । i i i i । a TTg i r » । t i i i । i i i • । Th m/z-> 40 50 60 70 80 90 100110120130140150160170180190 200 210 220230 Abundance #70788: Hexadecane ' .. * ..... 57 43 l-r 71 33.40 33.60 33.80 34.00 5000 85 m/z 85.05 42.56%

99 113 127 141 155 169 183 1 226 | ’ 1 । i । i i ii । i i ia । . i i i । • a a i । i k a । a i i i । i ii i। l1" • I i" " i" " r r "' i •" ' i miz-> 40 50 60 70 80 90 100 110120 130140150160170 180190 200 210 220 230 'Abundance #29267: Hexadecane 57 33.40 33.60 33.80 34.00 ' 71 m/z 55.10 28.07% 5000 85

m/z--> m p .. 'l .. 1134127,141.. 99 196 226 I" "I "I'I i'"' i" " i 40 50 60 70 80 90 100 110 120130 140 150 160 170 180 190 200 210 220 230 r'" i ■ ' ।A — 33.40 33.60 33.80 34.00 ■ i ■ ■ ■ ' i ■

26626.D NP112701.M Fri Dec 07 14:50:32 2001 Page 18

NYC-WTC_000031963

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