GCMS analysis results for sample AD26626, Dec 10 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26626.D Vial: 3 Acq On 6 Dec 2001 11:59 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 17 Tetracosane Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

32.80 0.87 ng/uL 196701 Chrysene-dl2 33.18

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane 338 C24H50 000646-31-1 (86 2 Heptadecane 240 C17H36 000629-78-7 80 3 Nonadecane 268 C19H40 000629-92-5 80 4 Heneicosane 296 C21H44 000629-94-7 72 Abundance Scan 3049 (32.798 min): 26626.D (-) m/z 57.10 100.00% i 57 43 71 5000 85 1 i ■ ' ■ ■ i ■ ■ ■ i ■ ■ 32.40 32.60 32.80 33.00 33.20 im/z-> _ .................................... ................................................... 1‘‘—11—‘111—TTTL""ITTET‘IITTTTET/"‘‘‘ITTT‘TITTEETCETETCTTE‘‘IT‘ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 m/z 43.10 65.23% Abundance #73543: Tetracosane i 43 57 71 / 5000 85 I I 32.40 32.60 32.80 33.00 33.20 1 ! 99 m/ Z 71'0.5 58.71% i m/z--> 40 — 60 113127 155169183197 Iit,' IT IJI TTTTTur T I'*•IjIt •I• i ■ ■111 294 338 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71191: Heptadecane 57 43 T 71 32.40 32.60 32.80 33.00 33.20 5000 m/z 85.05 39.09% 85

" 113127141 240 . '' I " " 11' •' I ‘ 1 I ’ ' TT I I ! | । . r । | i . I I | । • . < | ii > । TTIIT T‘ miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 — Abundance #71948: Nonadecane 43 57 32.40 32.60 32.80 33.00 33.20 m/ z 26.83% 71 5000 85

‘II — p-r d 99 113127 156 196210225 ■I •1 1 • 111 ‘TI‘‘‘11 268 i •1 ‘ ■ i ■ • ■ • i ■ ■ • ■ । 1111>i■■i ■ ■ ■11 1‘ i ' ■ ■ • । 1 ■ A I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00 33.20

26626.D NP112701.M Fri Dec 07 14:50:30 2001 Page 17

NYC-WTC_000031962