GCMS results log, sample AD26987, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26987.D Vial: 26 Acq On 7 Dec 2001 8:54 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 9 Tetracosane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

33.74 2.34 ng/uL 701358 Chrysene-dl2 33.18

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane 338 C24H50 000646-31-1(9 2 Hexadecane 226 C16H34 000544-76-3 '90 3 Heneicosane 296 C21H44 000629-94-7 90 4 Pentacosane 352 C25H52 000629-99-2 90 ■Abundance Scan 3152 (33.744 min): 26987.D (-) m/z " 100.00% 57 43 5000- 85 ' TTT » I » I I I I • I TTTTIT . i — 99 33.40 33.60 33.80 34.00 113127141155 TI’TTTTTTTT ‘TT 'T'1 ’’T i''' • i 226 r •111'1111'11 1111111 ‘111111111 m/z 43.10 67.87% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 71

5000 85 TT 33.40 33.60 33.80 34.00 ■ 99 m/z71.0566.42% 1 il 113127 155169183197 294 338 1111 TTTrL’ TT 11 ‘ (‘ I • ’ ‘' I •' ‘ ‘ I'' ‘' I I'''' I'''' I' *' • I'''' I 11 1 I i111111 m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #70787: Hexadecane 43 57 TT 71 33.40 33.60 33.80 34.00

1 5000 - m/z 85.15 42.98% 85 27 99 113127141155 226 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #72684: Heneicosane II 1 11 1 1 1 1T • i ■ ■ ■ ■ i • 43 V 33.40 33.60 33.80 34.00 m/z 55.10 25.42% 71 5000- 85

99 113127 155169183197211269 296 miz-> r•••i••••r 20 40 60 TT TT"TI-1-TT11""‘TTTTTTTTTTITTTT-TVCTTTTtrTrTTI1 TTTTTT 80 100 120 140 160 180 200 220 240 260 280 300 320 340 rr-T-p T-r 33.40 33.60 33.80 34.00 1 ' i ■

26987.D NP112701.M Tue Dec 11 14:52:58 2001 Page 9

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