GCMS results log, sample AD26987, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26987.D Vial: 26 Acq On . 7 Dec 2001 8:54 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 10 Eicosane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

34.66 1.48 ng/uL 442007 Chrysene-dl2 33.18

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 2 Heptadecane 240 C17H36 000629-78-7 90 3 Tridecane, 1-iodo- 310 C13H27I 035599-77-0 86 4 Heptacosane 380 C27H56 000593-49-7 86 Abundance Scan 3252 (34.661 min): 26987.D (-) m/ z 57.10 100.00% 57 43 71 5000- 85 f

—T 12113127141 ......... 207................................................ m/ Z 34.40 34.60 34.80 35.00 43.10 68.20% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #72323: Eicosane 43 57

71 ) 5000 PCMP 11 MPP 85 34.40 34.60 34.80 35.00 m/ Z 71.0,5 59.27% 98 113 127 141 I m/z-> 1 1 — 1 TTT 40 60 +" j! 80 100 120 140 160 180 200 220 240 260 280 300 282 ■ i ■ ’

Abundance #711 S3: Heptadecane 57 ...... . . , I* । i ,|,r-r-r-|-r i i i 71 34.40 34.60 34.80 35.00 5000- 85 m/z 85.05 38.17%

99 J 113 127 141 155 169 210 240 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44187: Tridecane, 1-iodo- TI / 57 34.40 34.60 34.80 35.00 43 m/ Z 55.10 24.56% 71

5000 85

99 113 135 183 - ,| 1| , ||, 155 I 310 A TT 1 ' I ' ' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 34.40 34.60 34.80 35.00

26987.D NP112701.M Tue Dec 11 14:53:00 2001 Page 10

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