GCMS results log, sample AD26987, Dec 11 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26987.D Vial: 26 Acq On 7 Dec 2001 8:54 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Heneicosane Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

35.54 1.23 ng/uL 313029 Perylene-dl2 37.27

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 2 Pentacosane 3 Octacosane 4 Triacontane Abundance Scan 3348 (35.541 min): 26987.D (-) 296 C21H44 352 C25H52 394 C28H58 422 C30H62 m/ z 57.10 000629-94-7 000629-99-2 000630-02-4 000638-68-6 83 100.00% 0 57

5000 85

4 A fr--IP i 113 35.20 35.40 35.60 35.80 141 207 281 ’ 'T1' - TT‘‘tt1‘—‘t1‘1r-E-""I1"TEIT‘1E10-TEIITTCTT"TTITETTTTETITTTT m/z 43.10 72.58% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #42201: Heneicosane 57

85 5000 35.20 35.40 35.60 35.80 m/z 71.05 64.75% 113141 # i | "‘",‘‘"T0-TTTOETEITEFTTTETT"T‘TTTT '1 * I' ’' ‘I 268 296 TTTTTTTTTTT m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73718: Pentacosane 43 I ’ ■ ■ ■ j ' ■ ■ ■ i ■

71 35.20 35.40 35.60 35.80 5000 m/ Z 85.0.5 48.81%

99 127 155 183 211 I' • ‘ * I 11''11'''111111111'1111'11 I'' " I'''1 I'''' I ’ " ' I' " ' I 1 1 1 ' I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74211: Octacosane A I ' 1 I ' 43 35.20 35.40 35.60 35.80 m/ Z 55.10 28.94% 71 5000-

99 , 127 155 183 211 364 ... 111.1 It ITTTTT I'||'l। । r, । . r. । 1′111′13 TII 11 m/z- 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 35.20 35.40 35.60 35.80

26987.D NP112701.M Tue Dec 11 14:53:03 2001 Page 11

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