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GC/MS analysis results for sample AD22652, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22652 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087274–000087302

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22652.D Vial: 11 Acq On : 28 Sep 2001 10:14 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Heneicosane Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 36.40 0.90 ug/1 129259 Perylene-dl2 37.29 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91 2 Tetratetracontane 619 C44H90 007098-22-8 91 3 Octadecane 254 C18H38 000593-45-3 91 4 Heptacosane 380 C27H56 000593-49-7 91 Abundance Scan 3416 (36.398 min): 22652. D (-) m/z 57.00 100.00% 57

85 5000-

36.00 36.20 36,40 36.60 36.80

TTfe-> 50 " i(^ " " 200 " 2^ " 300 " " 5^ " 5^ ' ‘ 6^ m/z 71.00 79763% I Abundance #42201: Heneicosane 7

85 5000 “n* 36.00 36.20 36.40 36.60 36.80 m/z 43.05 64.76% Hi , 2682^ tVz-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #61068: Tetratetracontane 57 ---- / -- - I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' 36.00 36.20 36.40 36.60 36.80 5000 Wz 85.05 50.61% 85

r-n-p f .il J. I .... I .. ... . .. m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #71561: Octadecane T 7 36.00 36.20 36.40 36.60 36.80 ■m/z 55700^ 23.02% 85 5000

m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 36.00 36.20 36.40 36.60 36.80

22652.D NP091101.M Wed Oct 03 11:53:33 2001 Page 15

NYC-WTC_000087295

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NYC-WTC_000087295Source: NYC Law Department, mirrored locally

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