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GC/MS analysis results for sample AD23320, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23320 conducted on October 15, 2001.

NYC-WTC_000088207–000088236

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088229
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT12 01\23320.D Vial: 13 Acq On : 12 Oct 2001 1:51 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ■ : 209 625/TCLP calibration table 7/16/01 Library : C:\DAT7kBASE\NBS75K.L ********************************************************************* Peak Number 16 Heneicosane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 35.50 3.78 ug/1 359103 Perylene-dl2 37.22 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91\ 2 Tetracosane 338 C24H50 000646-31-1 91 3 Hexatriacontane 507 C36H74 000630-06-8 91 / 4 Heptadecane ____________________ 240 C17H36 000629-78-7 ^bundance Scan 3318 (35.497 min); 23320.D (-) m/z 57.00 100.00% 57

5000 85

T-r-f-r-r-r-r-T J I I J 169 -197 225 253 281 ........... 35.20 35.40 35.60 35.80 m/z 71.00 71.22% ■nlz-> 50 100 150 200 250 300 350 400 450 500 Abundance #42201: Heneicosane 57

5000- 85 TT-p-T A 35.20 35.40 35.60 35.80 TT-p-r

in/z 43700 64.73% |113 wxi (j ...... ...................... ■nZz-> 50 100 150 200 250 300 350 400 450 500 Abundance #73543; Tetracosane 7

35.20 35.40 35.60 35.80 5000- 85 m/z 85.05 48.92% (i

I ilTi 155J83 294 , 3^............................................. ■n/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #59136: Hexatriacontane 5|7 35.20 35.40 35.60 35.80 Wz 55700 24.24%

5000 85

50 100 150 ■ 200 239 250 300 350 379 407 435 478 506 400 450 500 35.20 35.40 35.60 35.80 I 23320.D NP091101.M Mon Oct 15 09:54:05 2001 Page 16

NYC-WTC_000088229

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NYC-WTC_000088229Source: NYC Law Department, mirrored locally

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