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GC/MS analysis results for sample AD23321, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23321 conducted on October 15, 2001.

NYC-WTC_000088237–000088262

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088258
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23321.D Vial: 14 Acq On : 12 Oct 2001 2:50 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Heneicosane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 36.36 1.53 ug/1 166743 Perylene-dl2 37.23 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91 2 Hexatriacontane 507 C36H74 000630-06-8 91 3 Tetratetracontane 619 C44H90 007098-22-8 91 4 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 91 Abundance Scan 3411 (36.358 min): 23321 .D (-) m/z 57.00 10^700% 57

cWBW 85

36.00 36.20 36.40 36.60 r-r+ysY^-rr^-f-T^T'-f-YT-V-r-ry-rT-T-T-p-T-T-T-yT-T-rnq-T-TT-nryT-T-T-ryT-T-T-T-yT-^^ m/z TITOO 72.82% ■nfe-> 50 100 150 200 250 300 350 400 450 500 550 Hili] Abundance #42201: Heneicosane 5|7

85 552 36.00 36.20 36.40 36.60 43.05 64.31% .. J. .1 I.... I.... , ft tVz-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #59136: Hexatriacontane 7 A 36.00 36.20 36.40 36.60 5000 m/z 85705 50.10% 85

379407435 478506 ' ' I ' ' ' ' I ' ' ■n/z~> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #61068: Tetratelracontane 57 36.00 36.20 36.40 36.60 m/z 41.00 24714% 5000 85

f i* J. f/. u-! V??, I .... I .... I. .. I I. . 50 100 150 200 250 300 350 400 450 500 550 600 36.00 36.20 36.40 36.60

23321.D NP091101.M Mon Oct 15 10:22:43 2001 Page 14

NYC-WTC_000088258

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NYC-WTC_000088258Source: NYC Law Department, mirrored locally

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