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GC/MS analysis results for sample AD23321, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23321 conducted on October 15, 2001.

NYC-WTC_000088237–000088262

Folder label: “GC/MS Scan 9/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23321.D Vial: 14 Acq On : 12 Oct 2001 2:50 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L Peak Number 13 Tetratetracontane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 35.49 2.33 ug/1 254341 Perylene-dl2 37.23 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetratetracontane 619 C44H90 007098-22-8 9\ 2 Heneicosane 296 C21H44 000629-94-7 91\ 3 Tricosane 324 C23H48 000638-67-5 '91 / 4 Eicosane, 9-octyl-__________________ 394 C28H58 013475-77-9 91 Abundance Scan 3317 (35,495 min): 23321 ,D (-) m/z 5^795 100700% 57

85 5000 J T 35,20 35,40 35,60 35,80

Ti/z-> 50 .' .MJzf............. 100 150 200 250 300 350 400 450 500 550 600 m/z 71705 71.15% ^bundance #61068: Tetratetracontane 7

553 85 35.20 35,40 35,60 35,80 m/z 43.05 66.54%

Ti/z-> 50 100 Ci'J, f ............. 150 200 250 300 350 400 450 500 550 600 Abundance #42201: Heneicosane 57 T 35,20 35,40 35,60 35,80 85 m/z 85705 50713%

LWX ..... 268296................... mfe-> Abundance 50

43 100 150 200 250 300 350 400 #73318: Tricosane 450 500 550 600 A I ''111 35,20 35,40 35,60 35,80 m/z 55.00 26.92% 71 5000

99 107 ,'3 .tu I ■ . I., .... I.... .... . I..... T ■n/z-> 100 150 200 250 300 350 400 450 500 550 600 35,20 35,40 35,60 35,80

23321.D NP091101.M Mon Oct 15 10:22:41 2001 Page 13

NYC-WTC_000088257

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NYC-WTC_000088257Source: NYC Law Department, mirrored locally

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