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GC/MS analysis results for sample AD23499, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23499 conducted on October 19, 2001.

NYC-WTC_000088799–000088825

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088820
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NYC 9/11 Public Portal Document

Library-Search-Compound Report

Data File : C:\HPCHEM\1\DATA\OCT1601\23499.D Vial: 7 Acq On : 16 Oct 2001 8:06 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Tetratetracontane Concentration Rank 9 . R.T. EstConc Area Relative to ISTD R.T. 36.36 2.28 ug/1 240059 Perylene-dl2 37.24 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetratetracontane 619 C44H90 007098-22-8 91< 2 Heneicosane 296 C21H44 000629-94-7 '91 / 3 Heptacosane 380 C27H56 000593-49-7 91/ 4 Hexatriacontane 507 C36H74 000630-06-8 91/ Abundance Scan 3412 (36.364 min): 23499.D (-) m/z SYTOO 100.00% 57

5000 85

' I ' ' ' ' I 36,00 36,20 36,40 36,60 ,, 211 253281 m/z 7^/95 69702% m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #61068: Tetratetracontane 5)7

5000- 85 36,00 36,20 36.40 36,60 m/ z 43,0^ 61.75% . . 379407 590618 7l/Z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance - - #42201: Heneicosane 57

36,00 36,20 36,40 36,60 85 5000 m/z 85.05 45.85%

|113,.. - - J 268296 ■nfe-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance------- - #52248: Heptacosane _ — _ < I I I T l-r 57-- 36,00 36,20" 36,40 ~36,60 in/z ,54.95 23.04% 5000 85

380 -r-t-r-p-n-r-p- T(/Z-> 50 100 150 200 250 300 350 400 450 500 . 550 600 36,00 36,20 36,40 36,60

23499.D NP091101.M Thu Oct 18 10:14:35 2001 Page 15 NYC-WTC1000088820

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NYC-WTC_000088820Source: NYC Law Department, mirrored locally

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