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GC/MS analysis results for sample AD23499, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23499 conducted on October 19, 2001.

NYC-WTC_000088799–000088825

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088821
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NYC 9/11 Public Portal Document

-Library Search Compound-Report Data File : C:\HPCHEM\1\DATA\OCT1601\23499.D Vial: 7 Acq On : 16 Oct 2001 8:06 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table '7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 16 10-Methylnonadecane Concentration Rank 13 R.T. EstConc Area Relative. to ,ISTD R.T. 38.37 0.68 ug/1 71531 Perylene-dl2 37.24 Hit# of 5 Tentative ID MW MolForm CAS# Qual

10-Methylnonadecane 282 C20H42 000000-00-0 91 2 Pentatriacontane 493 C35H72 000630-07-9 90. 3 Nonacosane 408 C29H60 000630-03-5 90 4 Hexatriacontane 507 C36H74 000630-06-8 90 Abundance Scan 3630 (38.365 min); 23499.D (-) m/z 57700 100.00%! 5(7

5000

mfe-> Abundance 3.. ..1.4.4’ 85

" r "' I''" I"'' I"'' I''" I'" * I'''' I H I I I'•) I I I I I • I I I I • I I I I I I«« I I I I I I« I I I I I I I I I I I I I I• I I I I

40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 #39858:10-Methylnonadecane 281 X] 38.00 38.20 m/z71.00 38.40 38.60 65.36%

57

85 5000 38.00 38.20 38.40 38.60 154 "mTz 43700 56733% ,.,1... Li.jlX..., I mfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance-------------------------------------- —#58743; Pentatriaconlane——"* 57

38,00 38.20 38.40 38.60 5000 85 m/z 85.00 49.24%

i r. 11 169 197 225 j. A . jT. I I n 1111.1111 A - p ... 1111 > I H ,. I I " " I " " I " " I' " ' I " " I m/z-> 40 60 80 100 120 140160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance ------ - --- #54526: Nonacosane 43 -38.00 '38.20 - 38.40 38.60 ~ m/z 41700 27773% 71 Mt

m/z-> JjJuX 211 239 I' • •' I' I ‘i 11 r. 11) 11 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 . 379 408 . I'"' I ’I"' ‘ I" " I" ” I" " I"'' r .38.00 38.20 38.40 38.60

23499.D NP091101.M Thu Oct 18 10:14:37 2001 Page 16 NYC-WTC_000088821

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NYC-WTC_000088821Source: NYC Law Department, mirrored locally

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