GCMS analysis summary, sample AD31377, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1502\31377.D Vial: 23 Acq On : 16 Jan 2002 8:28 am Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Hexatriacontane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

36.08 1.49 ug/1 143722 Perylene-d12 36.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Pentadecane 212 C15H32 000629-62-9 80 3 Nonadecane 268 C19H40 000629-92-5 80 4 Tetratetracontane _________ 619 C44H90 _______ 007098-22-8 80 Abundance Scan 3381 (36.080 min): 31377.D (-) m/z 56.95 100.00% 43 57 71 85 5000

97 35.80 36.00 36.20 36.40 TT MW —113127 141 154 159 191 207 ..... m/z 43.05 95.74% miz-? 40 60 80 100 " 120 “ 140 " 160 ‘ ' 180 " 200 ' 220 " 240 " 260 ' Abundance #74636: Hexatriacontane 43 57

71 5000 85 35.80 36.00 36.20 36.40 m/z 71.10 73.36% I 97 113 127 141 155 169 183 197 211 +*I**’’I*’I’+* ■ i • ■ ‘ ■ i ■ ■ ' ■ i ■ ‘ ■ ■ i • ■ • • i ■ ■ ■ ■ i ■ ‘ • • i ■ ■ ■ ■ i • ■ ■ ■ i ‘ miz-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance es00t -sdenme 57 43 i 71 35.80 36.00 36.20 36.40 5000 85 m/z 85.05 58.36%

99 113 127 168 212 mfe-> 40 60 80 100 120 140 160 180 “ 200 220 ' 240 260 Abundance #37469: Nonadecane 43 57 71 35.80 36.00 36.20 36.40 m/z 41.05 36.56% 85 5000

■ ■ i ' ■ i 111111 , X, 113, ................ 268 , m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 35.80 36.00 36.20 36.40

31377.D GCMS1126.M Mon Feb 04 15:08:17 2002 Page 5

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