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GC/MS analysis results for sample AD23502, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23502 conducted on October 19, 2001.

NYC-WTC_000088880–000088904

Folder label: “GC/MS Scan 9/27/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File :.C:\HPCHEM\1\DATA\OCT1601\23502 .D Vial: 10 Acq On : 16 Oct 2001 11:02 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Hexatriacontane Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 36.37 1.28 ug/1 136515 Perylene-dl2 37.23 . Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 9K. 2 Heptadecane 240 C17H36 000629-78-7 91< 3 Tetratetracontane 619 C44H90 007098-22-8'90 4 Tetracosane 338 C24H50 000646-31-1 90 Abundance Scan 3412 (36.366 min); 23502.D (-) Wz 57700 107700% 57

5000 85

Il 1 2^3281 36 00 36.20 36.40 36.60 m/z 71705 68.18% Tife-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #74636; Hexatriacontane 57

5000 85 36.00 36.20 36.40 36.60 m/z4370565750%

7l/Z-> n-r-p 50 3^/................... -.......... 100 150 200 250 300 350 400 450 500 550 ,, 600 Abundance #32063; Heptadecane — 57-

85 36,00 36.20 36.40 36.60 5000 m/z 85.05 47.99% A I fr,141 196 240 Tife-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #61068; Tetratetracontane 5(7 36.00 36.20 36.40 36.60 - - ■m/z—55.00 26.-91%

5000- 85

I^ri^^t''?9lg7225 379407 590618 a/

■n/z-> 50 100 150 200 250 300 350 400 450 500 550 600 36.00 36.20 36.40 36.60

23502.D NP091101.M Thu Oct 18 10:25:12 2001 Page 15

NYC-WTC_000088901

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NYC-WTC_000088901Source: NYC Law Department, mirrored locally

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