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GC/MS analysis results for sample AD23502, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23502 conducted on October 19, 2001.

NYC-WTC_000088880–000088904

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088900
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

iribr’ary Search Compound Report Data File : C:\HPCHEM\i\DATA\OCT1601\23502.D Vial: 10 Acq On : 16 Oct 2001 11:02 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TGLP calibration table 7/16/01 Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Heneicosane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 35.50 2.20 ug/1 234884 Perylene-dl2 37.23 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 . . 000629-94-7 9T 2 Octadecane 254 C18H38 000593-45-3 91 3 Eicosane, 7-hexyl- 366 C26H54.. 055333-99-8 91 4 Heneicosane, 11-(1-ethylpropyl)- 366 C26H54 055282-11-6 91' Abundance Scan 3318 (35.504 min); 23502.D (-) mp 5776^ 100.00% 57 43 71 85 5000

99 .... R,.... 35.20 35.40 35.60 35.80 J, Jj T^r^^l 155169183197210 253 281 m/z 71.00 71791% ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #42201: Heneicosane 57 71 85 552 35.20 35.40 35.60 35.80 99 m/z 43.05 69.93%

Tife-> JU 268 296 'I ' ' “' I ' ' ' ' I ' ' ' ' I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 I I I f' ' I ' I

iKbundance #71561; Octadecane 57 43 71 I Till-, I I r, , , pT-i 35.20 35.40 35.60 35.80 85 5000 in/z 85.05 51.35%

99 X 224 254

A 1111 r 1111 I p . 111 I ' ' ' ’ I ’ ’ ' ' I n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #50999: Eicosane, 7-hexyl- T-r-p-T TT-p-T 43 57 35.20 35.40 _35.60 35.80___ m/z 55.00 -24.0 9%

5000 71 ft 85

'' I'' 11 ll 169182197 281 310 "'I""I"" I I (fApnpZp , <1 I'l I I I , I I Tlfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 35.20 35.40 35.60 35.80

23502.D NP091101.M Thu Oct 18 10:25:10 2001 Page 14

NYC-WTC_000088900

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NYC-WTC_000088900Source: NYC Law Department, mirrored locally

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