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GC/MS analysis results for sample AD23324, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.

NYC-WTC_000088316–000088345

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088339
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23324.D Vial: 17 Acq On : 12 Oct 2001 5:46 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 17 Heneicosane Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T. 36.36 3.81 ug/1 357203 Perylene-dl2 37.23 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91\ 2 Heneicosane, 11-(1-ethylpropyl)- 366 C26H54 055282-11-6 91\ 3 Heptacosane 380 C27H56 000593-49-7 91 / 4 Heptadecane, 9-octyl- 352 C25H52 007225-64-1 91 Abundance Scan 3412 (36.362 min): 23324.D (-) m/z 57.00 100.00% 57

85 5000

4

Ti/z-> Abundance XUh 11'^ J d 1®9 197 224 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 #42201: Heneicosane 253 281 I " " I ' " ' T ‘' I " " I " 36,00 36,20 36,40 36,60 m/z 71.10 69.73%

57

25S 85 I 36,00 36,20 36,40 36,60 m/z 43.05 67.83% 113 ,,,,

■n/z-> 444 '' I'' 4^ 268 296 I'''' I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #51002: Heneicosane, ll-(l-ethylpropyl)- 43 ' ■7' )• ■ . I ■ 1 I 1 I 1 1 ■ I I 1 71 36.00 36,20 36.40 36,60 5000 m/z 85.05 51.26%

183 225 295 338 I' •' • I " " I " " 1" " I' • " I " " J •' " I " " I' " ’ I " I'' ’ 11.1111 tVz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #52248: Heptacosane ' I ' ' ' ' I ' ' 57 36,00 36,20 36,40 36,60 m/z 55.00 23.28%

5000 85

j ijfl , 169 196 224 324 380 281 'I'"..... I" • • 11" " p " I " '' I'''' I Tl/2-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 36,00 36,20 36,40 36,60

23324.D NP091101.M Mon Oct 15 10:33:57 2001 Page 17

NYC-WTC_000088339

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NYC-WTC_000088339Source: NYC Law Department, mirrored locally

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