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GC/MS analysis results for sample AD23606, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23606 conducted on October 19, 2001.

NYC-WTC_000088961–000088985

Folder label: “GC/MS Scan 9/27/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23606.D Vial: 13 Acq On : 17 Oct 2001 1:59 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K;L ********************************************************************* Peak Number 14 Heneicosane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 35.50 1.58 ug/1 168190 Perylene-dl2 37.24 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91 2 Hexatriacontane 507 C36H74 000630-06-8 91aS 3 Heptadecane 240 C17H36 000629-78-7 91 A 4 Tetratetracontane 619 C44H90 007098-22-8 91X Abundance Scan 3318 (35.502 min): 23606.D (-) m/z 57.00 100.00% 57

43 71

5000 85 K TiZz-> Abundance mux 40 60 80 99 1^1,

100 120 140 160 180 200 220 240 260 280 300 #42201: Heneicosane .............. m/z 35.20 35.40 35.60 35.80 71.10 71.89%

A 71 85 5000 -r-r5=pT-r‘ 35.20 35.40 35.60 35.80 99 m/z 43.05 67.23% 127 141 155 A TTfe-> 40 60 JUU 80 100 120 140 160 180 200 268 296 T'-' " I " " I ' 220 240 260 280 300 Abundance #74636: Hexatriacontane -43-57

71 35.20 35.40 35.60 35.80 553 85 m/z 85.05 49.53%

97 r¥*p-T-TTq-TTn-T-|*T-T-T- ‘ryT-rTn-yT-T~rTjn^^ Tl/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71193: Heptadecane “1 I A| I " r I I I t I I I I I I _ 57__ :;22:35;2g_35;40_35W_35,80__ 55700 -24-775% 71 5000 85 — 99 , J 1^127141 155169 J 210 240 .................. I ' I ' ' ' ' I ' ' ' ' I nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 35.20 35.40 35.60 35.80

23606.D NP091101.M Thu Oct 18 10:36:08 2001 Page 14 .

NYC-WTC_000088981

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NYC-WTC_000088981Source: NYC Law Department, mirrored locally

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